Journal
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
Volume 140, Issue 33, Pages 10443-10446Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jacs.8b06957
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Funding
- UC Irvine
- National Institutes of Health [R35GM127071]
- National Science Foundation [CHE-1465263]
- NATIONAL INSTITUTE OF GENERAL MEDICAL SCIENCES [R35GM127071] Funding Source: NIH RePORTER
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We report a Rh-catalyzed hydrothiolation of 1,3-dienes, including petroleum feedstocks. Either secondary or tertiary allylic sulfides can be generated from the selective addition of a thiol to the more substituted double bond of a diene. The catalyst tolerates a wide range of functional groups, and the loading can be as low as 0.1 mol %.
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