Journal
JOURNAL OF SYNCHROTRON RADIATION
Volume 20, Issue -, Pages 711-720Publisher
INT UNION CRYSTALLOGRAPHY
DOI: 10.1107/S0909049513018621
Keywords
Extreme Conditions beamline (P02.2); PETRA III; high-pressure single-crystal diffraction; data collection; data reduction; Esperanto data format
Categories
Ask authors/readers for more resources
Fast detectors employed at third-generation synchrotrons have reduced collection times significantly and require the optimization of commercial as well as customized software packages for data reduction and analysis. In this paper a procedure to collect, process and analyze single-crystal data sets collected at high pressure at the Extreme Conditions beamline (P02.2) at PETRA III, DESY, is presented. A new data image format called 'Esperanto' is introduced that is supported by the commercial software package CrysAlis Pro (Agilent Technologies UK Ltd). The new format acts as a vehicle to transform the most common area-detector data formats via a translator software. Such a conversion tool has been developed and converts tiff data collected on a Perkin Elmer detector, as well as data collected on a MAR345/555, to be imported into the CrysAlis Pro software. In order to demonstrate the validity of the new approach, a complete structure refinement of boron-mullite (Al5BO9) collected at a pressure of 19.4 (2) GPa is presented. Details pertaining to the data collections and refinements of B-mullite are presented.
Authors
I am an author on this paper
Click your name to claim this paper and add it to your profile.
Reviews
Recommended
No Data Available