4.2 Article

Exploration of synchrotron Mossbauer microscopy with micrometer resolution: forward and a new backscattering modality on natural samples

Journal

JOURNAL OF SYNCHROTRON RADIATION
Volume 19, Issue -, Pages 814-820

Publisher

WILEY-BLACKWELL
DOI: 10.1107/S0909049512032414

Keywords

synchrotron Mossbauer microscopy; nuclear resonant incoherent X-ray imaging; meteorite; Fe-57 phantom; 5 mu m resolution

Funding

  1. Consortium for Materials Properties Research in Earth Sciences under NSF [EAR 06-49658]
  2. NIH in University of California, Davis [GM-65440]
  3. ANL [58927-30-132]
  4. US Department of Energy, Office of Science, Office of Basic Energy Sciences [DE-AC02-06CH11357]

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New aspects of synchrotron Mossbauer microscopy are presented. A 5 mu m spatial resolution is achieved, and sub-micrometer resolution is envisioned. Two distinct and unique methods, synchrotron Mossbauer imaging and nuclear resonant incoherent X-ray imaging, are used to resolve spatial distribution of species that are chemically and magnetically distinct from one another. Proof-of-principle experiments were performed on enriched Fe-57 phantoms, and on samples with natural isotopic abundance, such as meteorites.

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