Journal
JOURNAL OF SEPARATION SCIENCE
Volume 36, Issue 24, Pages 3889-3895Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.201300694
Keywords
Acrylamide; Carbon nanotubes; Electropolymerization; Food samples; Solid-phase microextraction
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Funding
- Fujian Key Projects of Science and Technology [2011YZ0001-1]
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We developed a solid-phase microextraction coupled to GC with electron-capture detection method for the detection of acrylamide in food samples. Single-walled carbon nanotubes and polypyrrole were electropolymerized onto a stainless-steel wire as a coating, which possessed a homogeneous, porous, and wrinkled surface, chemical and mechanical stability, long lifespan (over 300 extractions), and good extraction efficiency for acrylamide. The linearity range between the signal intensity and the acrylamide concentration was found to be in the range 0.001-1 g/mL, and the coefficient of determination was 0.9985. The LOD, defined as three times the baseline noise, was 0.26 ng/mL. The reproducibility for each single fiber (n = 6) and the fiber-to-fiber (n = 5) repeatability prepared in the same batch were less than 4.1 and 11.2%, respectively.
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