Journal
JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS
Volume 72, Issue 3, Pages 176-180Publisher
PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.jpcs.2010.12.003
Keywords
Semiconductors; Electron microscopy; Raman spectroscopy; X-ray diffraction; Optical properties
Funding
- National Nanotechnology Center (NANOTEC)
- National Science and Technology Development Agency (NSTDA)
- Ministry of Science and Technology
- Thailand Research Fund (TRF), Bangkok, Thailand
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Microwave-assisted synthesis is a novel method used to synthesize CdMoO4 nanoparticles in propylene glycol. The effects of reaction time and microwave power on phase, morphologies, and optical properties of CdMoO4 nanoparticles were studied, using X-ray diffraction (XRD). Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), and UV-visible spectroscopy. The present analyses proved that these crystalline powders were scheelite-type tetragonal structured CdMoO4, with the crystallite size of 14-20 nm, and 4.51-4.73 eV band gaps, controlled by the synthetic conditions. (C) 2010 Elsevier Ltd. All rights reserved.
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