Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 76, Issue 12, Pages 5123-5131Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo2008725
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Funding
- Japan Society for the Promotion of Sciences [21590124, 21790025]
- Grants-in-Aid for Scientific Research [21790025, 21590124] Funding Source: KAKEN
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The atropisomeric properties of seven-membered-ring benzolactams (7a-c and 8a) [1,5-benzodiazepin-2-one (a), 1,5-benzothiazepin-4-one (b), and 1-benzazepin-2-one (c)] were examined. The atropisomers were isolated as the diastereomers with an (S)-phenethylamide moiety, which were characterized by X-ray crystallography, and the barriers to their interconversion were clarified.
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