Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 76, Issue 19, Pages 8033-8035Publisher
AMER CHEMICAL SOC
DOI: 10.1021/jo201226g
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Funding
- Ministry of Science and Higher Education of Poland [NN204/1579/33]
- [DS/I18/10/2010]
- [DS/I19/7/2011]
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A novel method for measuring heavy-atom KIEs for magnetically active isotopes using H-1 NMR is presented. It takes advantage of the resonance split of the protons coupled with the heavy atom in the H-1 spectrum. The method is validated by the example of the C-13-KIE on the hydroamination of styrene with aniline, catalyzed by phosphine-ligated palladium triflates.
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