Journal
JOURNAL OF NATURAL PRODUCTS
Volume 71, Issue 11, Pages 1938-1941Publisher
AMER CHEMICAL SOC
DOI: 10.1021/np800226n
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Funding
- Shenyang Personnel Bureau
- Shenyang Science and Technology Bureau
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The first total synthesis of bulbophylol-B (1) has been achieved with the longest linear sequence of 12 steps and an overall yield of 17.9% via a new and practical approach to construct the dihydrodibenz[b,f]oxepin skeleton employing Wittig, selective reduction, and intramolecular Ullmann reactions as key steps.
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