Journal
JOURNAL OF MATERIALS SCIENCE
Volume 43, Issue 19, Pages 6414-6421Publisher
SPRINGER
DOI: 10.1007/s10853-008-2718-7
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Spark plasma sintering experiments were conducted on Zr- and Hf-based borides and carbides with the addition of 1, 3, and 9 vol% MoSi2 as sintering aid. For comparison, as-received ZrC, HfC, ZrB2, HfB2 powders were also sintered. The microstructural features were investigated by means of scanning electron microscop-energy dispersive spectroscopy technique. Silicon carbide was detected in all the doped compositions along with significant amounts of oxide species (Hf/ZrO2, and SiO2). The effect of the MoSi2 content on densification, microstructure, and mechanical properties is analyzed.
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