Journal
JOURNAL OF MACROMOLECULAR SCIENCE PART A-PURE AND APPLIED CHEMISTRY
Volume 51, Issue 5, Pages 441-446Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/10601325.2014.893142
Keywords
low reactive temperature; chitosan; Gold nanoparticles; green route
Categories
Funding
- Foundation of Science and Technology Department of Sichuan Province [2012FZ0131]
- State Key Laboratory of Oil and Gas Reservoir Geology and Exploitation (Southwest Petroleum University) [PLN1112, 1201]
- Science Foundation of Southwest Petroleum University [2012XJZ011]
- National Natural Science Foundation of China [51304166, 50903011]
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A green and facile method has been developed to prepare gold nanoparticles (Au NPs) coated by chitosan in aqueous solutions. Herein, Au NPs capped with chitosan which acted as both the reducing and stabilizing agents were prepared through a two-step route at low temperature. HAuCl4 and chitosan initially reacted for 6h at room temperature, and subsequently the mixture reacted for another 1hour at 35 degrees C. Ultraviolet visible spectroscopy, X-ray photoelectron spectroscopy, and X-ray diffraction spectroscopy results confirmed the presence of Au NPs. Transmission electron microscopy indicated that the nanoparticles were dispersed individually. The analysis of thermogravimetric analysis and Fourier transform infrared spectroscopy showed that chitosan was capped on the surface of Au NPs.
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