Journal
JOURNAL OF HETEROCYCLIC CHEMISTRY
Volume 46, Issue 2, Pages 317-319Publisher
WILEY-BLACKWELL PUBLISHING, INC
DOI: 10.1002/jhet.56
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A convenient and high-yielding synthesis of 2,3-dichloroquinoxalines from the corresponding 2,3-dihydroxyquinoxalines has been developed. Treatment of a slurry of the 2,3-dihydroxyquinoxaline 1a-j with N,N-dimethylformamide in the presence of excess thionylchloride in 1,2-dichloroethane results in the rapid and high-yielding formation of the 2,3-dichloroquinoxaline derivatives 2a-j. Simplified workup and purification procedures for these compounds are also described.
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