Journal
JOURNAL OF COORDINATION CHEMISTRY
Volume 63, Issue 8, Pages 1411-1417Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/00958971003754540
Keywords
Synthesis; Cyclotetramerization; 4; 5-Dichlorophthalonitrile; Microwave irradiation
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The synthesis of octakis(4,5-bis{2-[2-(1-naphthyloxy)ethoxy]ethoxy}) metal-free (4) and metallophthalocyanines (5-8) were carried out by the cyclotetramerization of a 4,5-bis{2-[2-(1-naphthyloxy)ethoxy]ethoxy}phthalonitrile (3). Newly substituted octakisphthalocyanines showed enhanced solubility in organic solvents. The new compounds were characterized by IR, 1H-NMR, 13C-NMR, UV-Vis, and MS spectral data.
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