Journal
JOURNAL OF COORDINATION CHEMISTRY
Volume 63, Issue 5, Pages 861-867Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/00958971003645953
Keywords
Phthalocyanine; Microwave; Phthalonitrile
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Dinitrile monomer (3) was synthesized by nucleophilic aromatic substitution of 4-phenoxyphenol (1) with 4-nitrophthalonitrile (2). The metal-free phthalocyanine (4) was prepared by the reaction of dinitrile monomer (3) with DMAE. Ni(II), Co(II), and Zn(II) metallophthalocyanines were prepared by the reaction of 3 with chlorides of Ni(II), Co(II), and Zn(II) in DMAE. The new compounds were characterized by IR, 1H- and 13C-NMR, UV-Vis, elemental analysis, and MS specral data.
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