Journal
JOURNAL OF CLUSTER SCIENCE
Volume 25, Issue 2, Pages 483-493Publisher
SPRINGER/PLENUM PUBLISHERS
DOI: 10.1007/s10876-013-0626-8
Keywords
Electrochemical reduction method; TiO2 nanoparticle; Three component reaction; Tetrahydrobenzo[b]pyran
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Funding
- UGC Major Research Project, New Delhi
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An electrochemical reduction method was used for the preparation of TiO2 nanoparticles in which agglomeration with formation of undesired metal powders is prevented by the presence of ammonium stabilizers. These synthesized nanoparticles were characterized by UV-Visible, XRD, SEM-EDS and TEM analysis techniques. These synthesized nanoparticles of TiO2 were tested as heterogeneous catalyst for the synthesis of tetrahydrobenzo[b]pyran derivative using three components reaction of aromatic aldehyde, dimedione and malononitrile by simply stirring at room temperature in a solvent free condition.
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