Journal
JOURNAL OF CARBOHYDRATE CHEMISTRY
Volume 27, Issue 3, Pages 188-199Publisher
TAYLOR & FRANCIS INC
DOI: 10.1080/07328300802071245
Keywords
nonreducing end; NBS; cyclic acetals; oxidation; nitrobenzoyl
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Methyl 6-O-p-nitrobenzoyl-beta-D-glucoside was synthesized by reacting methyl 4,6-O-p-nitrobenzylidine-beta-D-glucoside with N-bromosuccinimide (NBS). First, methyl beta-D-glucoside was converted into methyl 4,6-O-p-nitrobenzylidine-beta-D-glucoside with p-nitrobenzaldehyde. Later, methyl 4,6-O-p-nitrobenzylidine-beta-D-glucoside was opened oxidatively with NBS to give methyl 6-O-p-nitrobenzoyl-beta-D-glucoside.
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