Article
Food Science & Technology
Xinlei Wang, Lin Zhu, Xuebo Song, Si Jing, Fuping Zheng, Mingquan Huang, Shengbao Feng, Luzhong La
Summary: In this study, the terpenoids and norisoprenoids in Qingke Baijiu were investigated, revealing their main components and potential markers for differentiation and aging process.
FOOD SCIENCE AND HUMAN WELLNESS
(2023)
Article
Food Science & Technology
Yin Wang, Xian Wang, Yuanyuan Huang, Tianli Yue, Wei Cao
Summary: Headspace solid-phase microextraction coupled with gas chromatography-mass spectrometry and headspace gas chromatography-ion mobility spectrometry were used to analyze the volatile organic compounds from chilled chicken contaminated with Staphylococcus aureus during early storage. Differential metabolites and their possible biotransformation pathways were analyzed using the KEGG database. Orthogonal partial least squares discriminant analysis was applied to identify biomarkers associated with the early stage of chicken meat contamination with S. aureus.
Article
Biochemical Research Methods
Goncalo Figueiredo, Carina Pedrosa Costa, Joana Lourenco, Tania Caetano, Silvia M. Rocha, Sonia Mendo
Summary: Microbial metabolomics is used to analyze and understand the metabolites produced and released by microorganisms in specific conditions. This research aims to investigate the impact of culture media changes on the metabolic profile and production of biotechnologically relevant compounds in Pedobacter lusitanus NL19 and Pedobacter himalayensis MTCC 6384. The study identified 320 metabolites belonging to different chemical families and associated 80 metabolites with various metabolic pathways. The findings provide insights into how slight changes in culture media composition can affect microbial metabolism and have potential applications in metabolomics pipeline construction and biotechnology.
ANALYTICAL AND BIOANALYTICAL CHEMISTRY
(2023)
Article
Chemistry, Applied
Xuemei Tian, Fenghua Wu, Guoxin Zhou, Jian Guo, Xingquan Liu, Tao Zhang
Summary: In this study, the volatile compounds in non-infested and S. oryzae-infested brown rice were analyzed to identify potential markers and facilitate pest monitoring. A reliable method to distinguish between non-infested and S. oryzae-infested brown rice was discovered. The findings of this study lay a foundation for further research on the brown rice infestation mechanism and safe storage monitoring.
Article
Food Science & Technology
Goncalo Jasmins, Rosa Perestrelo, Jean Daniel Coisson, Patricia Sousa, Jose A. Teixeira, Matteo Bordiga, Jose S. Camara
Summary: A study aimed to identify characteristic molecular markers related to the authenticity of Italian fortified wines. The volatilomic fingerprint of popular Italian fortified wines was established using HS-SPME/GCMS. The identified compounds can be used as potential markers for the authenticity and genuineness of these wines, contributing to the identification of fraud or adulteration cases and ensuring quality and safety for consumers.
Review
Engineering, Chemical
Sandra Pati, Maria Tufariello, Pasquale Crupi, Antonio Coletta, Francesco Grieco, Ilario Losito
Summary: This review explores and discusses two main aspects related to quantitative analysis of volatile compounds in wines using HeadSpace Solid Phase Micro-Extraction Gas-Chromatography/Mass-Spectrometry (HS-SPME-GC/MS). Recent advances in multivariate optimization approaches and critical aspects related to quantification methods, including matrix effects and various quantification approaches, are highlighted.
Article
Biochemistry & Molecular Biology
Alejandra Chavez-Marquez, Alfonso A. Gardea, Humberto Gonzalez-Rios, Luz Vazquez-Moreno
Summary: The study validates an untargeted metabolomics approach and utilizes recursive analysis of data to obtain high-quality wine characterization results and identify potential biomarkers.
Article
Food Science & Technology
Yin Wang, Yuanyuan Huang, Ni Cheng, Haoan Zhao, Ying Zhang, Cailing Liu, Liangliang He, Tianchen Ma, Yankang Li, Wei Cao
Summary: This study used HS-SPME-GC-MS and chemometrics analyses to investigate the variation of volatile substances in jujube honey contaminated by Zygosaccharomyces rouxii. The results identified specific volatile components that can distinguish contaminated honey from uncontaminated honey. This research provides a theoretical basis for the rapid detection of honey decomposition caused by Z. rouxii, which can improve nutritional quality and reduce economic losses.
Article
Chemistry, Analytical
Wencui Kang, Hao Lin, Waqas Ahmad, Huanhuan Li, Quansheng Chen
Summary: A nano-composite colorimetric sensor array coupled with near infrared spectroscopy was developed for the determination of active constituents. The sensor array, composed of chemically responsive dyes doped metal-organic frameworks, showed sensitive interaction with different volatile markers. Chemometric methods were used to separate kombucha broth samples with different fermentation times, enabling the estimation of the chemical and physical properties of tea fermentation broth.
MICROCHEMICAL JOURNAL
(2023)
Article
Chemistry, Applied
Yi Chen, Pao Li, Luyan Liao, Yeyou Qin, Liwen Jiang, Yang Liu
Summary: The study utilized a combination of HS-GC-IMS and HS-SPME-GC-MS to investigate the changes in volatile organic compounds (VOCs) during the fermentation of Liuyang Douchi, identifying 115 VOCs with distinct patterns at different fermentation stages. The research identified 49 marker VOCs that could distinguish the fermentation stages of Douchi based on their composition, with different VOCs contributing to the unique aromas of Douchi at each stage of fermentation.
Review
Food Science & Technology
Maria Tufariello, Sandra Pati, Lorenzo Palombi, Francesco Grieco, Ilario Losito
Summary: This review provides a snapshot of the main multivariate statistical techniques and methods used to process data on wine volatile molecule concentrations. It also discusses their applications and advancements in related fields.
Article
Food Science & Technology
Yingjie Miao, Gaowei Hu, Xiaolong Sun, Yashi Li, Huanting Huang, Yongqian Fu
Summary: The flavor characteristics of Chinese bayberry alcoholic beverages, including fermented bayberry wine (FBW) and integrated bayberry wine (IBW), were evaluated using analytical techniques such as HS-SPME GC-MS and UHPLC Q-TOF. The volatile compounds and soluble profiles were analyzed using multidimensional statistical analysis, revealing significant differences between FBW and IBW. IBW exhibited higher levels of key flavor components, such as b-caryophyllene, ethyl octanoate, ethyl nonanoate, and ethyl decanoate, contributing to its strong bayberry aroma and fruity flavor. On the other hand, FBW had higher concentrations of ethyl acetate and octanoic acid, which contribute to its fermented flavor. Soluble sugars, amino acids, and anthocyanin pigment cyanidin 3-glucoside were also found to be present in higher levels in IBW. This study highlights the importance of further research on the flavor profiles, potential applications, and market value of IBW.
Article
Chemistry, Multidisciplinary
Artemis K. Toulaki, Eleni Bozinou, Vassilis Athanasiadis, Theodoros Chatzimitakos, George I. Mantanis, Vassilis G. Dourtoglou, Stavros I. Lalas
Summary: This study investigates the application of pulsed electric field (PEF) combined with wood chips to expedite the flavor aging process of Xinomavro red wine. It examines the impact of different wood chip species on sensory attributes and volatile compounds. The results highlight the potential of PEF treatment to enhance the quality parameters of red wine aging.
APPLIED SCIENCES-BASEL
(2023)
Article
Biochemistry & Molecular Biology
Adam Kowalczyk, Piotr Kus, Zvonimir Marijanovic, Carlo I. G. Tuberoso, Izabela Fecka, Igor Jerkovic
Summary: In this study, gas chromatography-mass spectrometry analysis was conducted to analyze the volatile organic compounds in the leaves of seven different mint taxa. Principal component analysis identified two groups of chemotypes and the safety of their use was evaluated.
Article
Environmental Sciences
Xiaofang Yang, Xinmeng Zhu, Wei Gao, Ruyuan Jiao, Shan Zhao, Jianwei Yu Dongsheng Wang, Dongsheng Wang
Summary: The study found that MVOCs in sludge treatment processes are the main source of nuisance odors in wastewater treatment plants, and low-temperature thermal drying treatment can increase the odor intensity and MVOCs concentration of sludge. There is a significant positive correlation between bacterial community structures and key MVOC odorants.
ENVIRONMENTAL POLLUTION
(2022)
Article
Biochemical Research Methods
Goncalo Figueiredo, Carina Pedrosa Costa, Joana Lourenco, Tania Caetano, Silvia M. Rocha, Sonia Mendo
Summary: Microbial metabolomics is used to analyze and understand the metabolites produced and released by microorganisms in specific conditions. This research aims to investigate the impact of culture media changes on the metabolic profile and production of biotechnologically relevant compounds in Pedobacter lusitanus NL19 and Pedobacter himalayensis MTCC 6384. The study identified 320 metabolites belonging to different chemical families and associated 80 metabolites with various metabolic pathways. The findings provide insights into how slight changes in culture media composition can affect microbial metabolism and have potential applications in metabolomics pipeline construction and biotechnology.
ANALYTICAL AND BIOANALYTICAL CHEMISTRY
(2023)
Review
Engineering, Chemical
Abdo Hassoun, Sandeep Jagtap, Guillermo Garcia-Garcia, Hana Trollman, Mirian Pateiro, Jose M. Lorenzo, Monica Trif, Alexandru Vasile Rusu, Rana Muhammad Aadil, Vida Simat, Janna Cropotova, Jose S. Camara
Summary: Food quality has gained attention recently due to increased demand for healthier and more nutritious food. Traditional approaches to determine food quality are time-consuming and destructive, necessitating the development of novel analytical techniques. Food Quality 4.0, which utilizes Industry 4.0 technologies, aims to achieve rapid and objective assessment of food quality. This article discusses the fundamentals and principles of Food Industry 4.0 technologies, reviews common techniques used for food quality determination, and highlights advancements made in analytical techniques in the era of Industry 4.0.
JOURNAL OF FOOD ENGINEERING
(2023)
Article
Cardiac & Cardiovascular Systems
Sara Lopes Fernandes, Ricardo Ladeiras-Lopes, Mariana Silva, Gualter Silva, Ines Cruz, Silvia O. Diaz, Antonio S. Barros, Francisca Saraiva, Rita Faria, Joao Almeida, Paulo Fonseca, Helena Goncalves, Marco Oliveira, Nuno Ferreira, Joao Primo, Ricardo Fontes-Carvalho
Summary: Coronary artery calcium score (CACS) is associated with an increased risk of atrial fibrillation (AF) recurrence, particularly when the score exceeds 100.
JOURNAL OF CARDIOVASCULAR COMPUTED TOMOGRAPHY
(2023)
Article
Food Science & Technology
Serkan Selli, Rosa Perestrelo, Hasim Kelebek, Onur Sevindik, Fabiano Travaglia, Jean Daniel Coisson, Jose S. Camara, Matteo Bordiga
Summary: The impact of Japanese beetles on the quality indicators of Nebbiolo and Erbaluce grapes, specifically their phenolic and volatile composition, was examined. The study revealed that grapes produced by plants attacked by Japanese beetles had higher levels of phenolic compounds compared to healthy plants. Similarly, the volatile composition of the affected grapes was also higher. The plants responded to the beetle attack by increasing the content of certain volatile compounds.
FOOD RESEARCH INTERNATIONAL
(2023)
Article
Food Science & Technology
Lorena Gonzalez-Gomez, Sonia Morante-Zarcero, Jorge A. M. Pereira, Jose S. Camara, Isabel Sierra
Summary: This study analyzed 33 samples of tea and herbal tea infusions purchased in Spain and Portugal and found that 64% of the samples were contaminated with atropine and scopolamine. White and green teas were more contaminated compared to black and other herbal teas. Among the 21 contaminated samples, 15 had concentrations above the maximum limit set by the EU Commission Regulation (0.2 ng/mL) for liquid herbal infusions.
Article
Oncology
Fernando Osorio, Antonio S. Barros, Barbara Peleteiro, Isabel Amendoeira, Jose Luis Fougo
Summary: In this study, we compared the outcomes of breast cancer among three age groups and found that older patients were more susceptible to suboptimal treatment and had a lower overall survival rate. This was not associated with the cancer itself, but rather with undertreatment. The study suggests that tumor characteristics and treatment compliance are better predictors of survival than chronological age.
Article
Cardiac & Cardiovascular Systems
Marta Leite, Francisco Sampaio, Francisca A. Saraiva, Silvia O. Diaz, Antonio S. Barros, Ricardo Fontes-Carvalho
Summary: Recently, HF guidelines have re-classified HF patients with LVEF between 41% and 49% as HFmrEF. The treatment of HFmrEF patients is often considered a grey zone due to the lack of RCTs exclusively conducted on this population. A network meta-analysis was conducted to compare the treatment effect of different medications in HFmrEF cardiovascular outcomes.
Article
Food Science & Technology
Goncalo Jasmins, Rosa Perestrelo, Jean Daniel Coisson, Patricia Sousa, Jose A. Teixeira, Matteo Bordiga, Jose S. Camara
Summary: A study aimed to identify characteristic molecular markers related to the authenticity of Italian fortified wines. The volatilomic fingerprint of popular Italian fortified wines was established using HS-SPME/GCMS. The identified compounds can be used as potential markers for the authenticity and genuineness of these wines, contributing to the identification of fraud or adulteration cases and ensuring quality and safety for consumers.
Article
Chemistry, Analytical
Jose S. Camara, Paulo Fernandes, Nelson Barros, Rosa Perestrelo
Summary: An accurate and selective method combining modified mu-QuEChERS procedure with LC-QqQMS was developed for quantification of PAT in commercial apple juices. This method reduced interference from the matrix and provided a quick analysis within 10 minutes. The method showed good linearity and high recovery for determination of PAT in apple juice.
Article
Chemistry, Analytical
Patricia Sousa, Irene Camacho, Jose S. Camara, Rosa Perestrelo
Summary: Researchers have developed a potential diagnostic method for breast cancer using SDS-PAGE and MALDI-TOF MS, which can distinguish between breast cancer patients and healthy individuals based on peptide ion biosignatures.
Review
Environmental Sciences
Shahida Anusha Siddiqui, Shubhra Singh, Nur Alim Bahmid, Douglas J. H. Shyu, Ruben Dominguez, Jose M. Lorenzo, Jorge A. M. Pereira, Jose S. Camara
Summary: This article provides a detailed study on the impact of polystyrene microplastics (PS-MPs) on the food chain and the environment, including their mechanism, degradation process, and toxicity. The accumulation of PS-MPs in organisms' different organs leads to various adverse reactions, affecting diverse elements in the food chain. The article emphasizes the importance of developing a precise and effective methodology for extracting and quantifying PS-MPs in food.
SCIENCE OF THE TOTAL ENVIRONMENT
(2023)
Review
Microbiology
Rita Almeida Teixeira, Claudia Silva, Antonio Carlos Ferreira, Diana Martins, Adelino Leite-Moreira, Isabel M. Miranda, Antonio S. Barros
Summary: Gestational diabetes, affecting 10% of pregnancies, has implications for both mother and child. This study reviewed the literature on the differences in microbiota composition between pregnant women with gestational diabetes and healthy pregnancies. The findings suggest that certain bacteria are more abundant in healthy pregnancies, while others are more abundant in gestational diabetes. The study also highlighted the potential of microbiome-targeted therapies for gestational diabetes.
Review
Food Science & Technology
Rosa Perestrelo, Yassine Jaouhari, Teresa Abreu, Mariangie M. Castillo, Fabiano Travaglia, Jorge A. M. Pereira, Jose S. Camara, Matteo Bordiga
Summary: Fortified wines from Mediterranean countries have high alcohol content to increase their shelf-life during long journeys. Marsala, Madeira, Port, and Sherry are famous fortified wines due to their high alcoholic content, sweet taste, and intense aromatic profile. This review provides an overview of the traditional vinification process and regulatory aspects of Italian, Portuguese, and Spanish fortified wines, as well as the volatile organic compounds (VOCs) that contribute to their aroma and the compounds found during oxidative aging.
Review
Chemistry, Analytical
Patricia Sousa, Laurentina Silva, Catarina Luis, Jose S. Camara, Rosa Perestrelo
Summary: Cancer is the second leading cause of death, causing nearly 10 million deaths in 2020. Early detection, appropriate treatment, and patient care can reduce the cancer burden and increase the chances of cure. Matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS) is a high-throughput analytical approach that helps identify potential cancer biomarkers for early detection, diagnosis, and tumor progression. This review provides an updated overview of proteome/peptidome research using MALDI-TOF MS, discusses the application of statistical analysis in oncology, and compares the pros and cons of MALDI-TOF MS with tandem mass spectrometry (MS/MS)-based proteomics.
Review
Oncology
Cristina V. V. Berenguer, Ferdinando Pereira, Jose S. Camara, Jorge A. M. Pereira
Summary: Prostate cancer is a highly heterogeneous tumor that can range from indolent to aggressive forms. Overtreatment of patients with prostate cancer can lead to significant burdens, while careful monitoring can help avoid these problems. Early detection and knowledge of modifiable risk factors are important for reducing cancer risk. Innovations in prostate cancer diagnostics and therapy are needed to overcome current limitations.