Journal
MONATSHEFTE FUR CHEMIE
Volume 146, Issue 6, Pages 969-972Publisher
SPRINGER WIEN
DOI: 10.1007/s00706-014-1395-2
Keywords
Henry reaction; Aldehyde; Nitroalcohol; Nitromethane; Ambersep 900 OH
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Funding
- UGC, India [41-206/2012/SR]
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A green protocol has been developed for the selective synthesis of beta-nitroalcohols using commercially available Ambersep 900 OH as reusable heterogeneous catalyst. The reaction between aldehyde and nitromethane was performed under solvent-free condition at room temperature within a short time (70-150 min) in the presence of 10 wt % of Ambersep 900 OH to produce corresponding nitroalcohols in high yield (72-91 %). After the reaction is over, the catalyst can be separated and reused (3 cycles) without appreciable loss in its activity. [GRAPHICS] R = aryl, alkyl
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