4.7 Article

In situ crack-healing behavior of Al2O3/SiC composite ceramics under cyclic-fatigue strength

Journal

Publisher

PERGAMON-ELSEVIER SCIENCE LTD
DOI: 10.1016/j.icheatmasstransfer.2009.03.014

Keywords

Al2O3/SiC composite; Heat-resistance; Crack healing; Cyclic-fatigue strength

Funding

  1. Association of International Education, Japan (AIEJ) [2002]
  2. Yokohama National University Prof Ando Lab [6/30/2002-9/27/2002]
  3. Grants-in-Aid for Scientific Research [2002] Funding Source: KAKEN

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Alumina/silicon carbide (Al2O3/SiC) composite ceramics were sintered and subjected to three-point bending. A semicircular surface crack 50-320 mu m in diameter was made on each sample. Crack-healing behavior was systematically studied, as a function of cyclic-fatigue strength, crack-healing temperature, healing time, and crack size, and the bending strength of the crack-healed sample from room temperature to 1500 degrees C were investigated. Four main conclusions were drawn from the present study. (1) Crack-healed Al2O3/SiC sample exhibited very high cyclic-fatigue limit of 700 MPa. (2) Al2O3/SiC composite ceramics have the ability to heal after cracking, from 1000-1400 degrees C. (3) The composite material can completely heal a 300 mu m diameter semi-elliptical crack (aspect ratio 0.8-0.9). (4) The heat-resistance limit for monotonic loading of the crack-healed sample goes up to 1300 degrees C, and similar to 68% of the samples fracture, outside the crack-healed zone in the testing-temperature range 600-1300 degrees C. From these test results, it can be concluded that Al2O3/SiC has an excellent crack-healing ability and that crack healing is a desirable technology for the structural integrity of Al2O3/SiC. (C) 2009 Elsevier Ltd. All rights reserved.

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