4.5 Article Proceedings Paper

X-Ray Detection by Using CVD Single Crystal Diamond Detector

Journal

IEEE TRANSACTIONS ON NUCLEAR SCIENCE
Volume 56, Issue 3, Pages 849-852

Publisher

IEEE-INST ELECTRICAL ELECTRONICS ENGINEERS INC
DOI: 10.1109/TNS.2008.2010705

Keywords

CVB diamond; diamond; diamond detectors; X-ray beam intensity monitor

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A number of diamond detectors, obtained by a two-step growing procedure by chemical vapour deposition (CVD) technique, have been grown on a low cost commercial high temperature high pressure (HTHP) Ib single crystal diamond. The first diamond layer is 15 mu m thick and heavily doped by boron. A 35 mu m thick layer of intrinsic high purity and high quality CVD diamond is then grown on top of the doped diamond. A metal contact (aluminium 100 nm thick) is deposited on top of the intrinsic diamond. One of these devices has been placed in the beam of the station 9.1 of Synchrotron Radiation Source at Daresbury laboratory (UK) and several tests have been performed to assess the linearity of responsivity as a function of the photon flux, the long term stability, and the response to the sudden onset of radiation. The device shows an excellent linearity and long term stability (tested in the order of hours), while the response to the onset of radiation have still to be understood. The results obtained can open up the path to the construction of extremely radiation hard devices to be exploited as X-ray beam monitor.

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Schmid, S. Schmuck, M. Schneider, P. A. Schneider, D. Schworer, G. Scott, M. Scott, D. Scraggs, S. Scully, M. Segato, Jaemin Seo, G. Sergienko, M. Sertoli, S. E. Sharapov, A. Shaw, H. Sheikh, U. Sheikh, A. Shepherd, A. Shevelev, P. Shigin, K. Shinohara, S. Shiraiwa, D. Shiraki, M. Short, G. Sias, S. A. Silburn, A. Silva, C. Silva, J. Silva, D. Silvagni, D. Simfukwe, J. Simpson, D. Sinclair, S. K. Sipila, A. C. C. Sips, P. Siren, A. Sirinelli, H. Sjostrand, N. Skinner, J. Slater, N. Smith, P. Smith, J. Snell, G. Snoep, L. Snoj, P. Snyder, S. Soare, E. R. Solano, V Solokha, A. Somers, C. Sommariva, K. Soni, E. Sorokovoy, M. Sos, J. Sousa, C. Sozzi, S. Spagnolo, T. Spelzini, F. Spineanu, D. Spong, D. Sprada, S. Sridhar, C. Srinivasan, G. Stables, G. Staebler, I Stamatelatos, Z. Stancar, P. Staniec, G. Stankunas, M. Stead, E. Stefanikova, A. Stephen, J. Stephens, P. Stevenson, M. Stojanov, P. Strand, H. R. Strauss, S. Strikwerda, P. Strom, C. Stuart, W. Studholme, M. Subramani, E. Suchkov, S. Sumida, H. J. Sun, T. E. Susts, J. Svensson, J. Svoboda, R. Sweeney, D. Sytnykov, T. Szabolics, G. Szepesi, B. Tabia, T. Tadic, B. Tal, T. Tala, A. Tallargio, P. Tamain, H. Tan, K. Tanaka, W. Tang, M. Tardocchi, D. Taylor, A. S. Teimane, G. Telesca, N. Teplova, A. Teplukhina, D. Terentyev, A. Terra, D. Terranova, N. Terranova, D. Testa, E. Tholerus, J. Thomas, E. Thoren, A. Thorman, W. Tierens, R. A. Tinguely, A. Tipton, H. Todd, M. Tokitani, P. Tolias, M. Tomes, A. Tookey, Y. Torikai, U. von Toussaint, P. Tsavalas, D. Tskhakaya, I Turner, M. Turner, M. M. Turner, M. Turnyanskiy, G. Tvalashvili, S. Tyrrell, M. Tyshchenko, A. Uccello, V Udintsev, G. Urbanczyk, A. Vadgama, D. Valcarcel, M. Valisa, P. Vallejos Olivares, O. Vallhagen, D. Van Eester, J. Varje, S. Vartanian, T. Vasilopoulou, G. Vayakis, M. Vecsei, J. Vega, S. Ventre, G. Verdoolaege, C. Verona, G. Verona Rinati, E. Veshchev, N. Vianello, E. Viezzer, L. Vignitchouk, R. Vila, R. Villari, F. Villone, P. Vincenzi, I Vinyar, B. Viola, A. J. Virtanen, A. Vitins, Z. Vizvary, G. Vlad, M. Vlad, P. Vondracek, P. de Vries, B. Wakeling, N. R. Walkden, M. Walker, R. Walker, M. Walsh, E. Wang, N. Wang, S. Warder, R. Warren, J. Waterhouse, C. Watts, T. Wauters, A. Weckmann, H. Wedderburn Maxwell, M. Weiland, H. Weisen, M. Weiszflog, P. Welch, N. Wendler, A. West, M. Wheatley, S. Wheeler, A. Whitehead, D. Whittaker, A. Widdowson, S. Wiesen, J. Wilkinson, J. C. Williams, D. Willoughby, I Wilson, J. Wilson, T. Wilson, M. Wischmeier, P. Wise, G. Withenshaw, A. Withycombe, D. Witts, A. Wojcik-Gargula, E. Wolfrum, R. Wood, C. Woodley, R. Woodley, B. Woods, J. Wright, J. C. Wright, T. Xu, D. Yadikin, M. Yajima, Y. Yakovenko, Y. Yang, W. Yanling, V Yanovskiy, I Young, R. Young, R. J. Zabolockis, J. Zacks, R. Zagorski, F. S. Zaitsev, L. Zakharov, A. Zarins, D. Zarzoso Fernandez, K-D Zastrow, Y. Zayachuk, M. Zerbini, W. Zhang, Y. Zhou, M. Zlobinski, A. Zocco, A. Zohar, V Zoita, S. Zoletnik, V. K. Zotta, I Zoulias, W. Zwingmann, I Zychor

Summary: The JET 2019-2020 scientific and technological programme made use of previous scientific and engineering work to achieve significant research results. The focus was on scenarios for high fusion power and alpha particle physics, consequences of long-term exposure to JET-ILW plasma, and the nuclear technology programme for maximum technological return.

NUCLEAR FUSION (2022)

Article Radiology, Nuclear Medicine & Medical Imaging

Application of a novel diamond detector for commissioning of FLASH radiotherapy electron beams

Gianluca Verona Rinati, Giuseppe Felici, Federica Galante, Alessia Gasparini, Rafael Kranzer, Giulia Mariani, Matteo Pacitti, Giuseppe Prestopino, Andreas Schuller, Verdi Vanreusel, Dirk Verellen, Claudio Verona, Marco Marinelli

Summary: This study investigated the flashDiamond (fD) detector prototype and validated its suitability for pulsed electron beam irradiation. It also compared the results with commercially available dosimeters and demonstrated the suitability of the fD detector for commissioning UH-DPP linac beams.

MEDICAL PHYSICS (2022)

Article Chemistry, Analytical

Novel Electrochemical Sensors Based on L-Proline Assisted LDH for H2O2 Determination in Healthy and Diabetic Urine

Mauro Tomassetti, Riccardo Pezzilli, Giuseppe Prestopino, Corrado Di Natale, Pier Gianni Medaglia

Summary: This paper presents a novel non-enzymatic modified glassy carbon (GC) sensor for hydrogen peroxide (H2O2) determination in healthy and diabetic human urine. The sensor is based on the (GC-Ag-paste)-catalytic proline-assisted LDH system, where LDH is attached to the glassy carbon using silver paste and proline is utilized to enhance the catalytic properties of LDH. The sensor exhibits high sensitivity and the proline-assisted LDH system effectively detects H2O2 in the urine samples.

SENSORS (2022)

Article Chemistry, Analytical

Fast Detection of Different Water Contaminants by Raman Spectroscopy and Surface-Enhanced Raman Spectroscopy

Salvatore Almaviva, Florinda Artuso, Isabella Giardina, Antonia Lai, Alessandra Pasquo

Summary: Fast monitoring of water quality is crucial for environmental management and protection. Raman spectroscopy and SERS have advantages such as no sample preparation, easy operation, and field applicability. This article explores their application in detecting various substances in liquid samples, as well as the use of the coffee-ring effect for pre-concentration of analytes, enabling fast and on-site detection of water pollutants.

SENSORS (2022)

Article Crystallography

New Voltammetric Sensor Based on LDH and H2O2 for L-Proline Determination in Red and White Wines

Mauro Tomassetti, Claudio Leonardi, Riccardo Pezzilli, Giuseppe Prestopino, Corrado Di Natale, Pier Gianni Medaglia

Summary: We have developed a simple, fast, and inexpensive voltammetric system for determining proline concentration. The system uses a non-enzymatic sensor and can accurately measure the concentration of proline in standard solutions and real samples. The method has been successfully applied to commercial wine samples.

CRYSTALS (2022)

Review Chemistry, Physical

Vertically Aligned Nanowires and Quantum Dots: Promises and Results in Light Energy Harvesting

Giuseppe Prestopino, Andrea Orsini, Daniele Barettin, Giuseppe Arrabito, Bruno Pignataro, Pier Gianni Medaglia

Summary: The synthesis of crystals with a high surface-to-volume ratio is crucial for advanced electronic devices and sensors. Vertical nanowires aligned with the substrate surface are the easiest way to achieve this. Wet chemistry methods for growing aligned nanowires and functionalizing their surfaces with quantum dots have been studied, and the best results in terms of photoconversion efficiencies have been obtained through slow multi-step local drop casting. Among the materials used, ZnO shows the most promise due to its piezo-phototronic effects.

MATERIALS (2023)

Article Chemistry, Analytical

A Direct Catalytic Ethanol Fuel Cell (DCEFC) Modified by LDHs, or by Catalase-LDHs, and Improvement in Its Kinetic Performance: Applications for Human Saliva and Disinfectant Products for COVID-19

Mauro Tomassetti, Riccardo Pezzilli, Claudio Leonardi, Giuseppe Prestopino, Corrado Di Natale, Luigi Campanella, Pier Gianni Medaglia

Summary: This study demonstrates that introducing nanostructured layered double hydroxides (LDHs) into the anode compartment can enhance the kinetic performance of a direct catalytic ethanol fuel cell (DCEFC). The calibration sensitivity of the method increases by 1.3-fold with the introduction of LDHs and even further in the presence of hydrogen peroxide. By modifying the fuel cell with enzyme catalase crosslinked on LDHs and in the presence of hydrogen peroxide, the calibration sensitivity increases by 8-times. This modification shows positive results in ethanol detection for analytical applications and can also improve the energy performance of a DCEFC.

BIOSENSORS-BASEL (2023)

Article Engineering, Multidisciplinary

Wurtzite nanowires strain control by DC electrical stimulation

Giuseppe Prestopino, Pier Gianni Medaglia, David Scarpellini, Sergio Bietti, Pietro Oliva, Salvatore Monteleone, Andrea Orsini, Daniele Barettin, Federica Caselli, Paolo Bisegna

Summary: Nanomechanics is a highly developed area of research that requires new theories to explain significant changes in material properties at the nanometer scale. This article presents a unique method to control electro-mechanical forces on quasi-1D nanostructures through static electric fields, enabling direct control of strain on GaAs nanowires grown on a substrate.

ENGINEERING SCIENCE AND TECHNOLOGY-AN INTERNATIONAL JOURNAL-JESTECH (2023)

Article Engineering, Biomedical

A diamond detector based dosimetric system for instantaneous dose rate measurements in FLASH electron beams

Marco Marinelli, Fabio di Martino, Damiano Del Sarto, Jake Harold Pensavalle, Giuseppe Felici, Luigi Giunti, Veronica De Liso, Rafael Kranzer, Claudio Verona, Gianluca Verona Rinati

Summary: A dosimetric system based on flashDiamond detector is proposed for measuring the instantaneous dose rate in ultra high dose rate electron beams. The system shows good signal to noise ratios and fast response time, enabling accurate measurements of absolute dose and instantaneous dose rate.

PHYSICS IN MEDICINE AND BIOLOGY (2023)

Article Engineering, Electrical & Electronic

Thin PDMS-on-Sacrificial-PCB Devices

Pier Gianni Medaglia, Christian Falconi, Riccardo Pezzilli, Giuseppe Prestopino, Nerio Andres Montoya, Claudio Leonardi, Usman Khan

Summary: In this study, a simple, cheap, and environmentally friendly method is proposed to address the challenge of mechanical release in PDMS devices, by using conventional printed circuit boards (PCBs) as sacrificial carriers. The thick and thermally conductive copper layer of the PCB serves as an excellent heat spreading plate, improving temperature uniformity and enabling pre-release electrical characterizations. The proposed approach simplifies the integration of PDMS with electronics and can be applied to other elastomers.

ACS APPLIED ELECTRONIC MATERIALS (2022)

Proceedings Paper Engineering, Electrical & Electronic

Time-dependent degradation of hydrogen-terminated diamond MESFETs

C. De Santi, L. Pavanello, A. Nardo, C. Veron, G. Verona Rinati, D. Cannata, F. Di Pietrantonio, G. Meneghesso, E. Zanoni, M. Meneghini

Summary: In this paper, the changes in electrical performance induced by operating time in hydrogen-terminated diamond MESFETs for high power and high frequency applications are discussed. It was found that the current flowing in the sample increases during the stress step, while the drain current decreases in the full experiment. The on-resistance increases and the threshold voltage shifts during the characterization phase. The time-dependent behavior is attributed to the creation of defects inside the structure. Furthermore, a decrease in electroluminescence was observed, indicating increased carrier-defect scattering.

TERAHERTZ, RF, MILLIMETER, AND SUBMILLIMETER-WAVE TECHNOLOGY AND APPLICATIONS XV (2022)

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