Journal
MACROMOLECULAR MATERIALS AND ENGINEERING
Volume 300, Issue 9, Pages 937-943Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/mame.201500090
Keywords
composites; curing of polymers; epoxy; fibers; reinforcement
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Epoxy-based fiber-matrix composites based on a single-component curing system with pot times >>two weeks are described. Bisphenol-A-diglycidyl ether and hexahydrophthalic anhydride were used as epoxy matrix precursors; 1,3-dicyclohexyl-3,4,5,6-tetrahydropyrimidinium carboxylate (6Cy-CO2) was used as latent pre-catalyst. Glass fiber-reinforced epoxy resins were obtained both via thermal curing under air and under vacuum-assisted resin infusion conditions. The high quality of the resulting composites and the absence of any air inclusion were confirmed by DSC and x-ray tomography. Rheological and kinetic data revealed that the 6Cy-CO2-based systems allow for an advanced processing and outrival commercial amine-based hardeners in terms of speed of curing.
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