Journal
HIGH PRESSURE RESEARCH
Volume 32, Issue 4, Pages 471-481Publisher
TAYLOR & FRANCIS LTD
DOI: 10.1080/08957959.2012.725729
Keywords
neutron scattering; ceramic proton conductor; high pressure research; pressure cells; high temperatures
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Funding
- Swiss National Science Foundation [200021-124812]
- European Union [042095]
- Office of Science, Office of Basic Energy Sciences, of the US Department of Energy [DE-AC02-05CH11231]
- Swiss National Science Foundation (SNF) [200021_124812] Funding Source: Swiss National Science Foundation (SNF)
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In this study, a simple high-temperature high pressure cell concept has been developed to enable neutron diffraction and quasi-elastic and inelastic neutron-scattering studies to be conducted on large-volume powder samples of ceramic proton conductors at pressures of up to 1 GPa and at temperatures of up to 770 K. Details of the cell are provided, along with the first experimental neutron diffractograms (at 0.62 GPa and 300 K), quasi-elastic neutron-scattering spectra (at 0.58 GPa and 770 K) and inelastic neutron spectra (at 0.75 GPa and 530 K) determined for samples of BaCe0.8Y0.2O3.
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