4.6 Article

The Effect of Ultrafine-Grained Microstructure on Creep Behaviour of 9% Cr Steel

期刊

MATERIALS
卷 11, 期 5, 页码 -

出版社

MDPI
DOI: 10.3390/ma11050787

关键词

creep-resistant 9% Cr steels; ultrafine grained materials; creep; electron back scatter diffraction

资金

  1. Czech Science Foundation [16-09518S]
  2. MEXT, Japan [26220909]

向作者/读者索取更多资源

The effect of ultrafine-grained size on creep behaviour was investigated in P92 steel. Ultrafine-grained steel was prepared by one revolution of high-pressure torsion at room temperature. Creep tensile tests were performed at 873 K under the initially-applied stress range between 50 and 160 MPa. The microstructure was investigated using transmission electron microscopy and scanning electron microscopy equipped with an electron-back scatter detector. It was found that ultrafine-grained steel exhibits significantly faster minimum creep rates, and there was a decrease in the value of the stress exponent in comparison with coarse-grained P92 steel. Creep results also showed an abrupt decrease in the creep rate over time during the primary stage. The abrupt deceleration of the creep rate during the primary stage was shifted, with decreasing applied stress with longer creep times. The change in the decline of the creep rate during the primary stage was probably related to the enhanced precipitation of the Laves phase in the ultrafine-grained microstructure.

作者

我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。

评论

主要评分

4.6
评分不足

次要评分

新颖性
-
重要性
-
科学严谨性
-
评价这篇论文

推荐

Article Materials Science, Multidisciplinary

In Situ Synchrotron X-ray Analysis: Application of High-Pressure Sliding Process to Ti Allotropic Transformation

Zenji Horita, Daisuke Maruno, Yukimasa Ikeda, Takahiro Masuda, Yongpeng Tang, Makoto Arita, Yuji Higo, Yoshinori Tange, Yasuo Ohishi

Summary: This study applied severe plastic deformation through high-pressure sliding on pure Ti to examine the allotropic transformation. It was found that straining by high-pressure sliding processing was effective in promoting phase transformation and maintaining the transformed phase, while the reverse transformation from omega phase to alpha phase is controlled by thermal energy.

MATERIALS TRANSACTIONS (2021)

Article Materials Science, Multidisciplinary

High Temperature Creep Behaviour of Cast Nickel-Based Superalloys INC 713 LC, B1914 and MAR-M247

Marie Kvapilova, Petr Kral, Jiri Dvorak, Vaclav Sklenicka

Summary: The study compared the creep properties of nickel-based superalloys, including creep behavior, fracture mode, and deformation mechanism. Results showed that MAR-M247 exhibited the best creep properties, followed by B1914 and INC713 LC. All three alloys met the requirements for high temperature components.

METALS (2021)

Article Materials Science, Multidisciplinary

Continuous high-pressure torsion of pure Al and Al-2 wt% Fe alloy using multi-wires

Takahiro Masuda, Shoichi Hirosawa, Zenji Horita

Summary: In this study, an earlier version of the continuous HPT (CHPT) process was further developed to simultaneously process two wires for grain refinement. The modified CHPT process using enlarged anvils achieved a grain size reduction in pure Al to around 1 μm and in the Al-2% Fe alloy to around 400 nm, with a tensile strength of 280 MPa and an equivalent strain of around 25 introduced through the process. The study suggests the feasibility of using multiple wires in the CHPT process when the anvil diameter is increased.

JOURNAL OF MATERIALS SCIENCE (2021)

Article Materials Science, Multidisciplinary

Synchrotron X-ray diffraction observation of phase transformation during annealing of Si processed by high-pressure torsion

Yoshifumi Ikoma, Terumasa Yamasaki, Takahiro Masuda, Yoshinori Tange, Yuji Higo, Yasuo Ohishi, Martha R. McCartney, David J. Smith, Zenji Horita

Summary: In situ observation using synchrotron X-ray diffraction was conducted to study the phase transformation in Si containing diamond-cubic and metastable phases during annealing. Metastable body-centred-cubic and hexagonal diamond phases were identified at different annealing temperatures, suggesting a phase transformation mainly from bc8 to hd during the process.

PHILOSOPHICAL MAGAZINE LETTERS (2021)

Article Materials Science, Multidisciplinary

Thermal creep fracture of a Zrl%Nb cladding alloy in the α and (α plus β) phase regions

Vaclav Sklenicka, Petr Kral, Kveta Kucharova, Marie Kvapilova, Jiri Dvorak, Lubos Kloc

Summary: The study aims to investigate the creep and fracture behavior of a sponge-based modified Zr1%Nb cladding alloy in the alpha-Zr and (alpha+beta)-Zr phase regions. Through constant load creep tests and metallographic analyses, it was found that there is a close relationship between creep deformation and fracture, with different final fracture modes and fracture strain values observed in different phase regions.

JOURNAL OF NUCLEAR MATERIALS (2021)

Article Materials Science, Multidisciplinary

Homogeneous Strain Introduction Using Reciprocation Technique in High-Pressure Sliding

Takahiro Masuda, Kazushige Fujimitsu, Kosei Sumikawa, Takahiro Kajita, Yongpeng Tang, Shoichi Hirosawa, Yoichi Takizawa, Manabu Yumoto, Yoshiharu Otagiri, Zenji Horita

Summary: This study investigates the strain distribution in the high-pressure sliding processing for rods of pure Al and an AZ61 alloy, revealing the preferential introduction of strain in an oblique direction and suggesting solutions for improving the homogeneous strain distribution.

METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE (2021)

Article Chemistry, Physical

Creep Resistance of S304H Austenitic Steel Processed by High-Pressure Sliding

Petr Kral, Jiri Dvorak, Vaclav Sklenicka, Zenji Horita, Yoichi Takizawa, Yongpeng Tang, Lubomir Kral, Marie Kvapilova, Pavla Roupcova, Jakub Horvath

Summary: Creep behavior of S304H austenitic steel improved significantly at 500 degrees C after high-pressure sliding (HPS) processing, but deteriorated at 600 degrees C and 700 degrees C. The creep behavior was found to be related to the thermal stability of the processed microstructure.

MATERIALS (2022)

Article Materials Science, Multidisciplinary

Successive Grinding and Polishing Effect on the Retained Austenite in the Surface of 42CrMo4 Steel

Jiri Pechousek, Erno Kuzmann, Rene Vondrasek, Anna Olina, Vlastimil Vrba, Lukas Kouril, Tomas Ingr, Petr Kral, Miroslav Mashlan

Summary: This study investigated low-alloy 42CrMo4 steels using various testing methods and found that grinding and polishing of metallographic samples has a significant impact on the final results.

METALS (2022)

Review Materials Science, Multidisciplinary

Nanomaterials by severe plastic deformation: review of historical developments and recent advances

Kaveh Edalati, Andrea Bachmaier, Victor A. Beloshenko, Yan Beygelzimer, Vladimir D. Blank, Walter J. Botta, Krzysztof Bryla, Jakub Cizek, Sergiy Divinski, Nariman A. Enikeev, Yuri Estrin, Ghader Faraji, Roberto B. Figueiredo, Masayoshi Fuji, Tadahiko Furuta, Thierry Grosdidier, Jeno Gubicza, Anton Hohenwarter, Zenji Horita, Jacques Huot, Yoshifumi Ikoma, Milos Janecek, Megumi Kawasaki, Petr Kral, Shigeru Kuramoto, Terence G. Langdon, Daniel R. Leiva, Valery Levitas, Andrey Mazilkin, Masaki Mito, Hiroyuki Miyamoto, Terukazu Nishizaki, Reinhard Pippan, Vladimir V. Popov, Elena N. Popova, Gencaga Purcek, Oliver Renk, Adam Revesz, Xavier Sauvage, Vaclav Sklenicka, Werner Skrotzki, Boris B. Straumal, Satyam Suwas, Laszlo S. Toth, Nobuhiro Tsuji, Ruslan Z. Valiev, Gerhard Wilde, Michael J. Zehetbauer, Xinkun Zhu

Summary: This article comprehensively reviews recent advances in the development of ultrafine-grained and nanostructured materials through severe plastic deformation and provides a brief history of this field. Severe plastic deformation methods have been effective in producing materials with advanced mechanical and functional properties, and the field of NanoSPD has experienced significant progress in the past two decades.

MATERIALS RESEARCH LETTERS (2022)

Article Materials Science, Multidisciplinary

Electrical conductivity characterized at varying strains in spiral cut high-pressure torsion discs

Evander Ramos, Takahiro Masuda, Zenji Horita, Suveen Mathaudhu

Summary: This study characterized the electrical conductivity of pure copper discs processed by HPT and found that the conductivity varied with strain in agreement with literature and expectations based on grain boundary evolution. The spiral conductivity testing method introduced in this study can improve the characterization of HPT materials in future studies.

MATERIALS LETTERS (2022)

Article Chemistry, Physical

Influence of Cryo-Processing and Post-SPD Annealing on Creep Behavior of CP Titanium

Jiri Dvorak, Petr Kral, Andrey G. Kadomtsev, Vladimir I. Betekhtin, Maria V. Narykova, Marie Kvapilova, Vaclav Sklenicka

Summary: The commercial purity of VT1-0 titanium was processed using the rolling process to obtain an ultrafine-grained microstructure. Static annealing after processing led to a significant decrease in creep properties. The control creep mechanisms were determined based on the value of steady-state creep rate. Titanium prepared at elevated and room temperatures exhibited higher creep strength compared to titanium prepared at cryo-temperatures. Post-SPD annealing resulted in a significant decrease in creep properties.

MATERIALS (2022)

Article Nanoscience & Nanotechnology

Characterization of creep properties and the microstructure of a service-exposed low alloy CrMoV steel steam pipe

Marie Kvapilova, Marie Ohankova, Petr Kral, Jiri Dvorak, Kveta Kucharova, Josef Cmakal, Vaclav Sklenicka

Summary: The effect of service degradation on the microstructure and creep properties of a 0.5%Cr-0.5%Mo-0.3%V steel steam pipe after 77,900 hours of accumulated service time was investigated. The results showed that the dispersion of fine vanadium carbides played a significant role in the high creep resistance of the steel. However, the coarsening of vanadium carbides during creep resulted in a weakening of the precipitation hardening and a decrease in creep resistance.

MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING (2022)

Article Chemistry, Physical

High Pressure Torsion of Copper; Effect of Processing Temperature on Structural Features, Microhardness and Electric Conductivity

Lenka Kuncicka, Michal Jambor, Petr Kral

Summary: By optimizing the fabrication method, copper components with both advantageous electric conductivity and favorable mechanical properties can be acquired. In this study, the effects of different deformation conditions on the structure and properties of copper were investigated. It was found that deformation under cryogenic conditions resulted in refined structure and improved mechanical and electric behaviors compared to deformation at room temperature.

MATERIALS (2023)

Article Materials Science, Multidisciplinary

Effect of severe plastic deformation on creep behaviour and microstructure changes of P92 at 923 K

P. Kral, J. Dvorak, V Sklenicka, T. Masuda, Y. Tang, Z. Horita, L. Kuncicka, K. Kucharova, M. Kvapilova, M. Svobodova

Summary: The creep behavior of P92 steel at 923 K deformed by rotary swaging (RS) and high-pressure torsion (HPT) was studied, revealing that both microstructures coarsen with increasing creep time and strain. Creep strain accelerates the coarsening, especially in the HPT-processed state, affecting the creep mechanism. RS-processed P92 steel showed faster creep rate and higher ductility compared to coarse-grained (CG) state, although at high stresses, it exhibited similar creep behavior to CG state.

KOVOVE MATERIALY-METALLIC MATERIALS (2021)

暂无数据