期刊
CATALYSIS SCIENCE & TECHNOLOGY
卷 6, 期 13, 页码 4733-4742出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c6cy00331a
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The synthesis of a triethoxysilyl functionalised Pd-PEPPSI-IPr complex prepared via azide-alkyne cycloaddition is described. The complex was immobilised onto silica gel and applied as a heterogeneous catalyst in the Negishi reaction. The catalyst was active in both batch and continuous flow operation and was particularly effective for the coupling of heteroaryl chlorides. Long-term continuous flow experiments demonstrated good catalyst activity over fifteen hours.
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