Article
Agriculture, Multidisciplinary
Min Hu, Yujie Ben, Ming Hung Wong, Chunmiao Zheng
Summary: An optimized method for the analysis of antibiotic residues in different food groups was developed, achieving good detection limits and recovery rates. The method has been successfully applied to the identification and quantification of antibiotic residues in common food products.
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
(2021)
Article
Food Science & Technology
Fabiola Paoletti, Stefano Sdogati, Carolina Barola, Danilo Giusepponi, Simone Moretti, Roberta Galarini
Summary: A multiclass method has been developed and validated for the determination of antimicrobial substances in eggs, covering sixty-three antibiotics from ten families. The method was successfully validated and applied to analyze 100 commercial egg samples, with only 3% containing residues of authorized substances below the relevant Maximum Residue Limits (MRLs).
Article
Food Science & Technology
Fulya Tasci, Hale Secilmis Canbay, Mahmut Doganturk
Summary: The study found antibiotic residues in non-compliant milk samples, suggesting that not all milk producers adhere to good veterinary practices.
Review
Infectious Diseases
Silvia Cruz Barros, Ana Sanches Silva, Duarte Torres
Summary: Veterinary drugs are commonly used in disease prevention and treatment. However, the abuse of antibiotics as growth promoters leads to the presence of antibiotic residues in animal-origin foods, posing a threat to food safety and antibiotic resistance. Monitoring the levels of antibiotic residues in food intended for human consumption is crucial for ensuring food safety.
Article
Chemistry, Analytical
Nick Sleegers, Alexander L. N. van Nuijs, Marco van den Berg, Karolien De Wael
Summary: The electrochemical detection of cephalosporins was studied, with focus on the impact of degradation on the electrochemical fingerprint. Changes in fingerprints were analyzed to understand degradation pathways and enrich the electrochemical information of cephalosporins.
ANALYTICAL CHEMISTRY
(2021)
Article
Food Science & Technology
Fabiola Paoletti, Stefano Sdogati, Carolina Barola, Danilo Giusepponi, Simone Moretti, Roberta Galarini
Summary: A two-procedure approach was developed for the detection and confirmation of antibiotic residues in honey, achieving satisfactory recovery factors and low coefficients of variation. The method performance was validated through participation in proficiency tests, demonstrating effectiveness in detecting residues in honey samples from local markets.
Article
Biochemistry & Molecular Biology
Harischandra Naik Rathod, Bheemanna Mallappa, Pallavi Malenahalli Sidramappa, Chandra Sekhara Reddy Vennapusa, Pavankumar Kamin, Udaykumar Revanasiddappa Nidoni, Bheemsain Rao Kishan Rao Desai, Saroja Narsing Rao, Paramasivam Mariappan
Summary: A quick, sensitive, and reproducible analytical method for the determination of 77 multiclass pesticides and their metabolites in Capsicum and tomato by gas and liquid chromatography tandem mass spectrometry was standardized and validated. The method showed good recovery rates and precision, making it suitable for analyzing vegetable samples collected from market and farm gates.
Article
Food Science & Technology
Sara Morello, Sabina Pederiva, Rosa Avolio, Giuseppina Amato, Simona Zoppi, Alessia Di Blasio, Maria Cesarina Abete, Cristina Casalone, Rosanna Desiato, Giuseppe Ru, Daniela Marchis
Summary: The EU has lifted restrictions on using non-ruminant processed animal proteins in aquafeed, with potential future permission for poultry and pig feed, while also evaluating potential hazards related to antibiotic residues. Monitoring studies have detected tetracyclines in processed animal proteins, raising concerns about exposure to antibiotic residues.
Article
Chemistry, Analytical
David Fabregat-Safont, Elisa Gracia-Marin, Maria Ibanez, Elena Pitarch, Felix Hernandez
Summary: The research on antibiotics occurrence in the aquatic environment has gained attention due to their potential negative effects, such as bacterial antibiotic-resistance. Antibiotic residues are not completely removed in wastewater treatment plants and end up in water bodies. Analytical methodologies are needed to determine antibiotics in influent and effluent wastewater for various purposes, such as environmental risk assessment and estimating removal efficiencies.
ANALYTICA CHIMICA ACTA
(2023)
Article
Biochemistry & Molecular Biology
Sunyeong Jang, Hyungju Seo, Hojin Kim, Hyoyoung Kim, Jongsung Ahn, Hyunjeong Cho, Sunghie Hong, Seunghwa Lee, Taewoong Na
Summary: A method for the rapid and quantitative analysis of 30 veterinary drugs in feed samples was developed and validated. The method showed good linearity and recovery rates, and can be used for screening residual multiclass veterinary drugs in feed samples.
Article
Environmental Sciences
Catherine Chemtai, Fredrick O. Kengara, Anastasiah N. Ngigi
Summary: This study evaluated the presence of antibiotics in the surface water and sediments of River Sosiani in Kenya. The results showed high prevalence of antibiotics, with 28 detected in water and 29 detected in sediments. Some of the antibiotics posed ecological risks. These findings are crucial for devising mitigation strategies.
ENVIRONMENTAL MONITORING AND ASSESSMENT
(2023)
Article
Agriculture, Multidisciplinary
Christine R. Casey, Wendy C. Andersen, Nicole T. Williams, Tara J. Nickel, Patrick R. Ayres
Summary: An analytical program has been developed and validated for multiclass, multiresidue residue analysis of veterinary drug compounds in game meats using LC-MS/MS. The method was found to accurately detect 112 veterinary drug residues in muscle samples with an average accuracy ranging from 95.6% to 101%, and can also be used as a qualitative screening method.
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY
(2021)
Article
Biochemical Research Methods
Carmen Mejias, Juan Luis Santos, Julia Martin, Irene Aparicio, Esteban Alonso
Summary: In this paper, a method for the determination of antibiotics and their metabolites in sewage sludge and agricultural soil was proposed. The method utilizes ultrasound-assisted extraction, dispersive solid-phase extraction clean-up, and liquid chromatography-tandem mass spectrometry. The method was validated and showed good accuracy and precision. The results revealed that macrolides and fluoroquinolones were the antibiotic classes found at the highest concentrations in all types of samples.
ANALYTICAL AND BIOANALYTICAL CHEMISTRY
(2023)
Article
Chemistry, Analytical
Hamed Sahebi, Amir Jouya Talaei, Elham Abdollahi, Fataneh Hashempour-Baltork, Somaye Vali Zade, Behrooz Jannat, Nafiseh Sadeghi
Summary: This research developed a method using functional imidazole-based ionic liquid-modified magnetic chitosan nanoparticles and UPLC-MS/MS for the simultaneous pre-concentration and determination of twenty-two antibiotics and their metabolites in milk samples. The synthesized nanoparticles were characterized, and experimental variables were optimized. The proposed method showed good linearity and minimized matrix effects, with high recoveries and low limits of detection. Residual antibiotics were found in a significant number of milk samples, but the human health risks from milk consumption were found to be negligible.
Article
Biochemical Research Methods
David Fabregat-Safont, Elena Pitarch, Lubertus Bijlsma, Ionut Matei, Felix Hernandez
Summary: The accurate quantification of amoxicillin and related penicillins in water was addressed in this study using direct injection of samples and mass spectrometric detection. The methodology was validated and applied to different water matrices, detecting the presence of ampicillin and cloxacillin in specific water samples.
JOURNAL OF CHROMATOGRAPHY A
(2021)
Article
Food Science & Technology
Malgorzata Gbylik-Sikorska, Andrzej Posyniak, Tomasz Sniegocki, Bartosz Sell, Anna Gajda, Anna Sawicka, Monika Olszewska-Tomczyk, Tomasz Bladek, Grzegorz Tomczyk, Jan Zmudzki
FOOD AND CHEMICAL TOXICOLOGY
(2016)
Article
Chemistry, Analytical
Bartosz Sell, Tomasz Sniegocki, Jan Zmudzki, Andrzej Posyniak
JOURNAL OF ANALYTICAL TOXICOLOGY
(2018)
Article
Biochemical Research Methods
Jolanta Flieger, Malgorzata Tatarczak-Michalewska, Anna Kowalska, Anna Madejska, Tomasz Sniegocki, Anna Sroka-Bartnicka, Monika Szymanska-Chargot
JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES
(2017)
Article
Biochemistry & Molecular Biology
Jolanta Flieger, Anna Swiech-Zubilewicz, Tomasz Sniegocki, Joanna Dolar-Szczasny, Magdalena Pizon
Article
Biochemistry & Molecular Biology
Tomasz Sniegocki, Bartosz Sell, Marta Giergiel, Andrzej Posyniak
Article
Biochemistry & Molecular Biology
Tomasz Sniegocki, Bartosz Sell, Andrzej Posyniak
Article
Agriculture, Dairy & Animal Science
Lidia Radko, Tomasz Sniegocki, Bartosz Sell, Andrzej Posyniak
Article
Biochemistry & Molecular Biology
Marta Tikhomirov, Blazej Pozniak, Tomasz sniegocki
Summary: The study developed a sensitive and reliable HPLC analytical method for determination of buprenorphine in rabbit plasma, resulting in high repeatability and reproducibility. The method was tested in a pilot pharmacokinetic study in rabbits, confirming its suitability for comprehensive description of buprenorphine pharmacokinetics.
Article
Biochemistry & Molecular Biology
Marta Tikhomirov, Tomasz Sniegocki, Blazej Pozniak
Summary: This study investigated the impact of lipid presence on the performance of fentanyl detection in rabbit plasma. While fentanyl was reliably detected in both normal and lipemic plasma, the solvent extraction method showed differences in accuracy between the two matrices.
Article
Environmental Sciences
Bartosz Sell, Tomasz Sniegocki, Marta Giergiel, Andrzej Posyniak
Summary: This study investigated suspected poisoning cases of white-tailed eagles in Poland and found at least one anticoagulant rodenticide in their liver samples. The extensive use of rodenticides poses a high risk to white-tailed eagles in Poland.
Article
Medicine, General & Internal
Jolanta Flieger, Tomasz Sniegocki, Joanna Dolar-Szczasny, Wojciech Zaluska, Robert Rejdak
Summary: This study investigated the presence of BPs in the aqueous humor of patients undergoing cataract surgery for the first time. The results showed the presence of BPA and two structural isomers in the samples, with higher levels found in patients with coexisting ocular pathologies. Further research is needed to understand the consequences of BPs accumulation in the aqueous humor.
JOURNAL OF CLINICAL MEDICINE
(2022)
Article
Veterinary Sciences
Tomasz Sniegocki, Marta Giergiel, Bartosz Sell, Andrzej Posyniak
JOURNAL OF VETERINARY RESEARCH
(2018)
Article
Ecology
Jordan D. Phelps, Caroline G. Strang, Malgorzata Gbylik-Sikorska, Tomasz Sniegocki, Andrzej Posyniak, David F. Sherry
Article
Veterinary Sciences
Tomasz Sniegocki, Malgorzata Gbylik-Sikorska, Andrzej Posyniak
JOURNAL OF VETERINARY RESEARCH
(2017)
Article
Veterinary Sciences
Malgorzata Gbylik-Sikorska, Andrzej Posyniak, Tomasz Sniegocki, Bartosz Sell, Anna Gajda, Grzegorz Tomczyk, Jan Zmudzki
JOURNAL OF VETERINARY RESEARCH
(2016)