Kilo-Scale Electrochemical Oxidation of a Thioether to a Sulfone: A Workflow for Scaling up Electrosynthesis
出版年份 2022 全文链接
标题
Kilo-Scale Electrochemical Oxidation of a Thioether to a Sulfone: A Workflow for Scaling up Electrosynthesis
作者
关键词
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出版物
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume -, Issue -, Pages -
出版商
American Chemical Society (ACS)
发表日期
2022-07-01
DOI
10.1021/acs.oprd.2c00111
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注意:仅列出部分参考文献,下载原文获取全部文献信息。- Development of a Practical and Greener Process for the Dual Leucine Zipper Kinase Inhibitor GDC-0134 Comprising Two SNAr Reactions, Oxidation and Suzuki Coupling
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- (2022) Cassie Pratley et al. CHEMICAL REVIEWS
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- (2021) Nasser Amri et al. CHEMICAL RECORD
- Electrochemically driven desaturation of carbonyl compounds
- (2021) Samer Gnaim et al. Nature Chemistry
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- (2021) Richard C. D. Brown CHEMICAL RECORD
- Cathodic Corrosion of Metal Electrodes—How to Prevent It in Electroorganic Synthesis
- (2021) Tom Wirtanen et al. CHEMICAL REVIEWS
- Technological Innovations in Photochemistry for Organic Synthesis: Flow Chemistry, High-Throughput Experimentation, Scale-up, and Photoelectrochemistry
- (2021) Laura Buglioni et al. CHEMICAL REVIEWS
- Sulfoxide and Sulfone Synthesis via Electrochemical Oxidation of Sulfides
- (2021) Jin Kyu Park et al. JOURNAL OF ORGANIC CHEMISTRY
- Flow Electrosynthesis of Sulfoxides, Sulfones, and Sulfoximines without Supporting Electrolytes
- (2021) Nasser Amri et al. JOURNAL OF ORGANIC CHEMISTRY
- A Continuous-Flow Electrochemical Taylor Vortex Reactor: A Laboratory-Scale High-Throughput Flow Reactor with Enhanced Mixing for Scalable Electrosynthesis
- (2021) Ashley Love et al. ORGANIC PROCESS RESEARCH & DEVELOPMENT
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- Benzylic Photobromination for the Synthesis of Belzutifan: Elucidation of Reaction Mechanisms Using In Situ LED-NMR
- (2021) Yining Ji et al. JOURNAL OF ORGANIC CHEMISTRY
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- (2016) Georg Manolikakes et al. SYNTHESIS-STUTTGART
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- (2008) K. Chandrasekara Pillai et al. JOURNAL OF HAZARDOUS MATERIALS
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