Article
Materials Science, Multidisciplinary
Dong Hee Lee, Sang-Hoon Kim, Hyun Ji Kim, Byoung Gi Moon, Young Min Kim, Sung Hyuk Park
Summary: The extrusion speed has a significant impact on the microstructure and tensile properties of the AZXWMM91100 alloy. As the extrusion speed increases, the grain size gradually increases, leading to a decrease in tensile strength and a fluctuation in elongation.
METALS AND MATERIALS INTERNATIONAL
(2021)
Article
Nanoscience & Nanotechnology
R. G. Li, H. R. Li, H. C. Pan, D. S. Xie, J. H. Zhang, D. Q. Fang, Y. Q. Dai, D. Y. Zhao, H. Zhang
Summary: This study found that ultra-high strength can be obtained in a simple binary Mg-Gd alloy with a small extrusion ratio. This is mainly attributed to the strong texture and internal dislocation pinning in the un-dynamically recrystallized region. Furthermore, aging precipitation only occurs within the large un-DRXed grains, leading to a significant increase in tensile yield strength. Thus, the ultra-high strength of this alloy is mainly related to texture strengthening and precipitation strengthening.
SCRIPTA MATERIALIA
(2021)
Review
Chemistry, Physical
Yuan Qi Li, Feng Li, Fu Wei Kang, Hua Qiu Du, Zi Yu Chen
Summary: Extrusion process is a main method for forming lightweight and low plastic magnesium alloy components. New processes and methods are constantly emerging and applied to solve the long-term bottlenecks that restrict the rapid development of magnesium alloy extrusion forming technology. It provides scientific guidance and technical reserves for accelerating the development of magnesium and its alloys' deep processing technology, and expands the application range of high value-added magnesium alloy products.
JOURNAL OF ALLOYS AND COMPOUNDS
(2023)
Article
Nanoscience & Nanotechnology
Y. J. Wan, Y. Zeng, Q. Zeng, B. Song, X. F. Huang, X. Y. Qian, B. Jiang
Summary: By intentionally transforming the habit planes of lath-shaped Mg2Sn precipitates in Mg-Sn alloy from basal plane to prismatic plane, the strength and toughness of the alloy were significantly enhanced, with the compressive yield strength (CYS) and compression to failure (CF) increasing by 137% and 75% respectively. This was attributed to the significant obstacle effect of the abundant prismatic laths on basal slip and twinning.
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
(2021)
Article
Materials Science, Multidisciplinary
Yuanxiao Dai, MengHan Xiao, Yaobo Hu, Yan Yang, Bin Jiang, Tianxu Zheng, Li Dong, Baoqing Yang, Changyong Zheng
Summary: By designing extrusion parameters, the Mg-0.12Ca-0.08Ba alloy underwent grain refinement and texture control, resulting in the best performance of the extruded samples with different crystallographic orientations.
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
(2022)
Article
Metallurgy & Metallurgical Engineering
Mahdi Shiri, Hassan Jafari, Raman Singh
Summary: This review investigates the influence of extrusion parameters on the bio-corrosion performance of magnesium alloys. Dynamic recrystallization and grain refinement during extrusion can improve the mechanical properties and corrosion resistance of magnesium alloys. Increasing the extrusion ratio and decreasing the extrusion temperature can further enhance the bio-corrosion resistance of magnesium alloys.
TRANSACTIONS OF NONFERROUS METALS SOCIETY OF CHINA
(2022)
Article
Materials Science, Multidisciplinary
Hong Ning, Cheng Wang, Lu Xu, Shi Liu, Kai Zhang, Xiao-Li Zhou, Hui-Yuan Wang
Summary: This work systematically investigates the relevance between static recrystallization and pre-aging precipitates in AZ61 alloy and reveals that pre-aging precipitates can accelerate the initial recrystallization but gradually retard the recrystallization kinetics as the annealing time prolongs.
JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
(2022)
Article
Nanoscience & Nanotechnology
Yunhe Zheng, Laure Bourgeois, Jian-Feng Nie
Summary: This study investigated the structure of precipitates in Mg-Zn-Al alloys, revealing new structural features and proposing that the rod-shaped precipitates can be described by tiling of different shapes.
SCRIPTA MATERIALIA
(2021)
Article
Materials Science, Multidisciplinary
Cesar Palacios-Trujillo, Jose Victoria-Hernandez, David Hernandez-Silva, Dietmar Letzig, Marco A. Garcia-Bernal
Summary: This study investigated the superplastic behavior at intermediate temperatures of a commercial ZK60 magnesium alloy processed by indirect extrusion, showing a refined and homogeneous microstructure and achieving a very high ductility at 250 degrees C and 10(-4) s(-1). Grain boundary sliding (GBS) was concluded to be the dominant deformation mechanism based on calculations of the activation energy and interpretation of the deformation mechanism map for magnesium alloys.
Article
Nanoscience & Nanotechnology
Lili Guo, Jianqiang Wang, Xinbing Yun, Zhongchun Chen
Summary: This study developed novel Al clad Mg composites through continuous extrusion method, showing good metallurgical bonding between the Al shell and Mg core even without preheating of the Mg alloy. The fine-grained microstructure contributed to a significant enhancement in ultimate flexural strength (UFS) to 452 MPa. Preheating of the Mg alloy resulted in complete dynamic recrystallization (DRX) and modified texture of the Mg alloy, leading to a significant improvement in the bendability of the Al/Mg composite.
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING
(2021)
Article
Chemistry, Physical
Dongfang Lou, Mingda Zhang, Jinze Lv, Boxuan Li, Xiuwei Wang, Jianhua Shi, Yuping Ren, Hongxiao Li, Gaowu Qin
Summary: Indirectly extruded Zn-0.2Mg-(0, 0.05, 0.2, 0.4 wt%)Fe alloy rods exhibited improved ductility without sacrificing strength with the addition of minor Fe. The texture variation and grain refinement contributed to the enhancement of ductility and slight increase in strength. Increasing Fe content from 0.05 wt% to 0.4 wt% resulted in a reduction in elongation while maintaining yield strength and ultimate tensile strength.
JOURNAL OF ALLOYS AND COMPOUNDS
(2022)
Article
Metallurgy & Metallurgical Engineering
Zhiwei Du, Yonggang Peng, Hang Teng, Zhong Cao, Kui Zhang, Minglong Ma, Xiaolei Han, Ting Li, Cong Che, Yongjun Li
Summary: Crystal structures, growth characteristics, and transformation of the precipitates in a Mg-7Gd-5Y-1Nd-2Zn-0.5Zr (wt.%) alloy aged at 200 degrees C were investigated. The study revealed the formation and development of solute clusters and various precipitates during aging, providing valuable insights into the aging behavior and performance of the alloy.
JOURNAL OF MAGNESIUM AND ALLOYS
(2023)
Article
Materials Science, Multidisciplinary
Jae-Yeon Kim, Ki-Tae Yoo, Jai-Won Byeon
Summary: In this study, the effects of discontinuous precipitate (DP) and continuous precipitate (CP) on the tensile elongation and fracture mechanism of aging-treated AZ91D Mg alloy were investigated. The increase in area fraction of DPs was found to cause a slight decrease in tensile elongation due to cracking along grain boundaries. Experimental results also showed that a large number of fine tension twins were produced within a few percent of tensile elongation for specimens with high CP/alpha-Mg interfaces per unit volume, leading to premature fracture.
MATERIALS CHARACTERIZATION
(2021)
Article
Chemistry, Physical
Jian Qin, Hiromi Nagaumi, Chengbin Yu, Fangzhen Liu, Yifeng Li, Linsheng Wang
Summary: The temperature and time dependence of the radii of Mg2Si precipitates in 6082 Al alloy were investigated. The type of precipitating phase was determined using DSC and XRD. A thermodynamic model was designed to predict the evolution of particle size during the cooling process, which showed good agreement with experimental data. These findings provide guidance for optimizing the heat treatment process of alloys.
JOURNAL OF ALLOYS AND COMPOUNDS
(2022)
Article
Materials Science, Multidisciplinary
Inga G. Ringdalen, Ingvild J. T. Jensen, Calin D. Marioara, Jesper Friis
Summary: During aging, 6xxx aluminum alloys develop a microstructure with needle-shaped Mg/Si-rich precipitates in the bulk and larger Mg/Si-rich precipitates on the grain boundary, which play a role in intergranular fracture. The exact mechanisms of the grain boundary precipitates in intergranular fracture are still not fully understood. Various techniques, including Transmission Electron Microscopy and Density Functional Theory simulations, are used to study the structures and properties of these precipitates.
Article
Chemistry, Physical
Hiroyuki Watanabe, Yasuyoshi Sasakura, Naoko Ikeo, Toshiji Mukai
JOURNAL OF ALLOYS AND COMPOUNDS
(2015)
Article
Materials Science, Multidisciplinary
Toru Nagaoka, Yoshihisa Kimoto, Hiroyuki Watanabe, Masao Fukusumi, Yoshiaki Morisada, Hidetoshi Fujii
MATERIALS & DESIGN
(2015)
Article
Materials Science, Multidisciplinary
Jan Romberg, Jens Freudenberger, Hiroyuki Watanabe, Juliane Scharnweber, Andy Eschke, Uta Kuehn, Hansjoerg Klauss, Carl-Georg Oertel, Werner Skrotzki, Juergen Eckert, Ludwig Schultz
Article
Materials Science, Multidisciplinary
Takane Motoyama, Hiroyuki Watanabe, Naoko Ikeo, Toshiji Mukai
Article
Nanoscience & Nanotechnology
Hidetoshi Somekawa, Hiroyuki Watanabe, Dudekula Althaf Basha, Alok Singh, Tadanobu Inoue
SCRIPTA MATERIALIA
(2017)
Article
Metallurgy & Metallurgical Engineering
Hiroyuki Watanabe, Takane Motoyama, Naoko Ikeo, Toshiji Mukai
JOURNAL OF THE JAPAN INSTITUTE OF METALS AND MATERIALS
(2018)
Article
Materials Science, Multidisciplinary
Hiroyuki Watanabe, Masao Fukusumi
JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE
(2014)
Article
Materials Science, Multidisciplinary
Naoko Ikeo, Hiroki Kawasaki, Hiroyuki Watanabe, Toshiji Mukai
Article
Materials Science, Multidisciplinary
Hiroyuki Watanabe, Naoko Ikeo, Toshiji Mukai
MATERIALS TRANSACTIONS
(2019)
Article
Materials Science, Multidisciplinary
Hidetoshi Somekawa, Dudekula Althaf Basha, Alok Singh, Tomohito Tsuru, Hiroyuki Watanabe
PHILOSOPHICAL MAGAZINE LETTERS
(2020)
Article
Chemistry, Physical
Hiroyuki Watanabe, Toru Murata, Shunsuke Nakamura, Naoko Ikeo, Toshiji Mukai, Koichi Tsuchiya
Summary: Cold-working was found to facilitate the formation of sigma phase in CrMnFeCoNi alloy under specific heat treatment conditions. The resulting sigma-body-centered cubic (BCC) aggregates consist of sigma phase spines and BCC particles, forming rapidly at the face-centered cubic/sigma interface.
JOURNAL OF ALLOYS AND COMPOUNDS
(2021)
Article
Materials Science, Multidisciplinary
Hiroyuki Watanabe, Toru Murata, Naoko Ikeo, Toshiji Mukai, Kwangsik Han, Koichi Tsuchiya
Summary: The microstructural changes and flow behavior of a six-component high-entropy alloy were investigated under hot compression at 1173K. Results showed that the thermomechanically processed alloy with dense dispersion of second phases displayed steady-state flow and achieved finer grains compared to the homogenized alloy.
Article
Materials Science, Multidisciplinary
Alok Singh, Takanobu Hiroto, Hiroyuki Watanabe, Naoko Ikeo, Toshiji Mukai, Koichi Tsuchiya
Summary: Addition of Al to equiatomic high entropy alloy promotes formation of BCC phase and sigma phase. Straining by caliber rolling induces morphological changes related to planar faults, where sigma phase nucleates first on the matrix faults followed by formation of B2 phase driven by elemental concentration changes. This study provides insights into the formation mechanisms of different phases in the alloy.
MATERIALS CHARACTERIZATION
(2021)
Article
Materials Science, Multidisciplinary
Hiroyuki Watanabe, Yuya Takeuchi, Toshiji Mukai
Summary: Biodegradable magnesium-based composites have gained attention due to their biocompatibility and the ability to modify their mechanical and corrosion properties. This study investigated the effects of the fraction and crystal structure of tricalcium phosphate (TCP) on the electrochemical and mechanical properties of Mg-Ca/TCP composites. High-strength composites with a fine-grained matrix were prepared and exhibited compressive yield strengths exceeding 290 MPa. The electrochemical tests showed that the corrosion parameters were not affected by the fraction and crystal structure of TCP particles.
Article
Materials Science, Multidisciplinary
Hidetoshi Somekawa, Kimiyoshi Naito, Hiroyuki Watanabe