期刊
MATERIALS LETTERS
卷 142, 期 -, 页码 184-188出版社
ELSEVIER
DOI: 10.1016/j.matlet.2014.11.163
关键词
Magnetic iron oxides particles; Microwave-assisted synthesis; Low-temperature magnetic modification; Immobilized enzymes
资金
- Grant Agency of the Czech Republic [13-13709S]
- Ministry of Education, Youth and Sports of the Czech Republic [LD13021]
- Ministry of Education, Youth and Sports of the Czech Republic (Operational Program Research and Development for Innovations - European Development Fund) [CZ.1.05/2.1.00/03.0058]
Nano- and microparticles consisting of magnetic iron oxides were prepared by microwave-assisted synthesis from ferrous sulfate. They were applied to the direct magnetic modification of sensitive and labile non-magnetic biomaterials (such as plant and seagrass based materials and enzymes immobilized on non-magnetic carriers) at temperatures -20 and -80 degrees C. These conditions warrant stable magnetic modification of non-magnetic biomaterials, e.g. cellulose, lignocellulose, or starch based ones. We have also magnetically modified enzymes immobilized on non-magnetic carriers, for example lipase immobilized on cellulose powder and glucose isomerase immobilized on solid carrier granules. It was observed that a substantial fraction of the activity is maintained by this method and that all the magnetically modified enzymes were stable during eight repeated reaction cycles with only a negligible decrease in activity over time. (C) 2014 Elsevier B.V. All rights reserved.
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