期刊
GREEN CHEMISTRY
卷 12, 期 5, 页码 767-771出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/b925620b
关键词
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资金
- Department of Science & Technology, New Delhi [SR/S1/OC-49/2006]
- CSIR, New Delhi
An efficient, mild and rapid procedure for the acylation and alkylation of aromatic and aliphatic thiols mediated on a silica gel surface at room temperature is described. The protocol allows the protection of thiols under neutral heterogeneous conditions without requiring any bases or Lewis acids, and the silica gel used as the promoter can be recycled for several runs without any loss of activity.
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