期刊
GREEN CHEMISTRY
卷 11, 期 6, 页码 863-867出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/b820901d
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资金
- Polish Committee for Scientific Research [2 P06D 001 29]
The preparation of ylidenemalononitriles via Knoevenagel condensations of ketones with malononitrile under solvent-free conditions is described. Good yields and short reaction time are the features observed with methanesulfonic acid (MSA)/morpholine used as the catalyst. The wide applicability of the protocol is shown by the fact that not only unconjugated, but also aryl-alkyl ketones gave satisfactory yields.
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