期刊
FORENSIC SCIENCE MEDICINE AND PATHOLOGY
卷 5, 期 1, 页码 39-43出版社
HUMANA PRESS INC
DOI: 10.1007/s12024-008-9069-1
关键词
Cyanide; Blood; Determination; Head-space; Gas chromatography; Forensic toxicology
A method describing determination of cyanide in blood by head-space gas chromatography with electron capture detector was reported. The method involves transformation of cyanide into cyanogen chloride by reacting hydrogen cyanide with chloramine-T on a stick of filter paper in the space above the blood in the head-space vial. The recovery was 84-96% and the coefficient of variation was 3.3-7.2%. The limit of quantitation was about 0.01 mg cyanide/l.
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