期刊
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
卷 137, 期 36, 页码 11614-11617出版社
AMER CHEMICAL SOC
DOI: 10.1021/jacs.5b07860
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资金
- UCSB
- Amgen
- Junta de Castilla y Leon
- Fondo Social Europeo
- NIH Shared Instrumentation Grant [1S10OD012077-01A1]
The synthesis of sterically hindered anilines has been a significant challenge in organic chemistry. Here we report a Cu-catalyzed radical addition with in situ-generated nitroso compounds to prepare sterically hindered amines directly from readily available materials. The transformation is conducted at room temperature, uses abundant copper salts, and is tolerant of a range of functional groups.
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