The [M3L3](3+) metallo-macrocycles with syn, syn, syn conformation, self-assembled fromcrown ether functionalized 1,10-phenanthroline Pd(II) nitrates with naphthanoimidazole, bind a solvent CH3CN within the naphthanoimidazolate-built cavity through C-H center dot center dot center dot pi interactions in the crystalline state.
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