期刊
CRYSTENGCOMM
卷 14, 期 10, 页码 3677-3683出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c2ce06707b
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资金
- National Natural Science Foundation of China [20671003, 20971003]
- Chinese Ministry of Education [209060]
- Program for New Century Excellent Talents in University [NCET 11-0888]
- Science and Technological Fund of Anhui Province for Outstanding Youth [10040606Y32]
- Foundation of Key Project of Natural Science of Anhui Education Committee [KJ2012A143]
- Anhui Normal University
Twinned-hemisphere-like CuO architectures with sizes ranging from 2 to 2.5 mu m have been successfully prepared via a simple hydrophilic polymer-assisted hydrothermal route. The morphology of CuO is greatly affected by the mass ratio of Cu(CH3COO)(2)center dot H2O : PSS and the quantities of NaF. The different morphological products, such as spheres, twinned-hemispheres and sheets, have been obtained by changing the reaction conditions, which have been discussed in detail in this paper. The as-obtained products were characterized by SEM, XRD, FT-IR and BET. The adsorption capacity of the twinned-hemisphere product was detected by UV-vis spectroscopy. It was found that the as-obtained CuO twinned-hemispheres show high selectivity and short removal times to separate dyes from wastewater with a low cost and no secondary pollution.
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