期刊
COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS
卷 392, 期 1, 页码 264-270出版社
ELSEVIER
DOI: 10.1016/j.colsurfa.2011.10.003
关键词
Silver; Photoreduction; Tyrosine; Nanoparticles; Laser; UV irradiation
In this report we demonstrate a green chemical approach for the synthesis of stable silver nanoparticles in aqueous medium using tyrosine as an efficient photoreducing agent. A narrow size distribution of silver nanoparticles can be achieved by this simple photoirradiation method without using any additional stabilizing agents or surfactants. Two different irradiation sources have been explored resulting in a different particle size distribution pattern in each case. Further, we show that starting from a polydisperse tyrosine synthesized silver nanoparticles sample, it is also possible to fractionate them into different size ranges. The size fractionation was achieved by a 2 stage phase transfer method employing different organic solvents. The nanoparticles synthesized were characterized using UV-vis spectroscopy, Transmission electron microscopy (TEM) and X-ray diffraction (XRD) techniques. (C) 2011 Elsevier B.V. All rights reserved.
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