期刊
JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS
卷 375, 期 -, 页码 217-226出版社
ELSEVIER
DOI: 10.1016/j.jmmm.2014.09.044
关键词
Polyethyleneimine (PEI); Magnetic Nanoparticle; Spiro-oxindole; Pyrano[3,2-c]chromene; Surface functionalization
资金
- research council of Tehran University of Medical Sciences and Health Services
- Iran National Science Foundation (INSF)
A novel magnetically separable catalyst was prepared based on surface modification of Fe304 magnetic nanoparticle (IVINPs) with polyethyleneimine (PEI) via covalent bonding. 13-(2,3-Epoxypropoxy)propyl] trimethoxysilane (EPO) was used as cross linker to bond PEI on the surface of MNPs with permanent stability in contrast to PEl coating via electrostatic interactions. The synthesized catalyst was characterized by Fourier transform infrared (FT-IR), thermogravimetric analysis (TGA). X-ray powder diffraction (XRD), transmission electron microscopy (TEM) and vibrating sample magnetometry (VSM). The catalyst show high efficiency for one-pot synthesis of 2-amino-3-cyano 4/1 pyran derivatives via multi-component reaction (MCR). This procedure offers the advantages of green reaction media, high yield, short reaction time, easy purification of the products and simple recovery and reuse of the catalyst by simple magnetic decantation without significant loss of catalytic activity. (C) 2014 Elsevier B.V. All rights reserved,
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