期刊
CHINESE JOURNAL OF CHEMISTRY
卷 31, 期 8, 页码 983-986出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/cjoc.201300341
关键词
semiconducting material; synthesis; iron sulfide; Fe7S8; solvent-free
资金
- National Natural Science Foundation of China [20871041, 0903033, 21203053, 21271064]
- Joint Talent Cultivation Funds of NSFC-HN [U1204214]
- New Century Excellent Talents in University [NCET-08-0659]
- Scientific Research Foundation of Henan University [SBGJ090510, B2010079]
Employing green and economic solvent-free synthesis route, hexagonal iron sulfide (Fe7S8) nanoflowers were successfully synthesized for the first time. In the experiment, ferric hexadecylxanthate was used as the precursor, and hexagonal iron sulfide (Fe7S8) nanoflowers were obtained by thermal decomposition of the precursor at 260 degrees C without any additional solvent or inert gas protection. The as-prepared iron sulfide nanoflowers were characterized by means of X-ray diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM) and energy dispersive spectrometry (EDS). The characterization results indicated that the nanoflowers had uniform size distribution with an average size of about 160 nm. The proposed strategy provides a possible general route for the synthesis of other metal chalcogenide nanostructures.
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