期刊
CHEMISTRY-A EUROPEAN JOURNAL
卷 20, 期 40, 页码 12750-12753出版社
WILEY-V C H VERLAG GMBH
DOI: 10.1002/chem.201402303
关键词
bromination; bromine; microreactors; photoreactions
资金
- Ministry of Education, Culture, Sports, and Technology (MEXT) of Japan [2105]
- Grants-in-Aid for Scientific Research [26248031, 23241074, 24550213, 21106008] Funding Source: KAKEN
The photobromination of C-H bonds by using molecular bromine was reinvestigated under microfluidic conditions. The continuous-flow method suppressed the production of dibrominated compounds and effectively produced the desired monobrominated products with high selectivity. Rapid bromination of benzylic substrates containing a photoaffinity azide group was achieved without any decomposition.
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