期刊
CHEMICAL COMMUNICATIONS
卷 50, 期 36, 页码 4714-4716出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cc00851k
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资金
- Indonesian Ministry of National Education
The synthesis and resolution of a class of chiral organic fluorophores, axially chiral 4,4-difluoro-4-bora-3a,4a-diaza-s-indacenes (Ax*-BODIPY), is described. Ax*-BODIPYs were prepared through a modular synthesis combined with a late stage Heck functionalisation. Resolution was achieved by preparative chiral HPLC. Absolute stereochemical assignment was performed by comparison of experimental ECD spectra with TD-DFT calculations.
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