期刊
CHEMICAL COMMUNICATIONS
卷 50, 期 68, 页码 9718-9721出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c4cc04282d
关键词
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资金
- Natural Science Foundation of China [21172162, 21372174]
- Young National Natural Science Foundation of China [21202113]
- PhD Programs Foundation of Ministry of Education of China [2013201130004]
- Key Laboratory of Organic Synthesis of Jiangsu Province [KJS1211]
- PAPD
- Soochow University
A metal-free method for direct C(sp(3))-H bond functionalization of simple ethers with alpha,alpha-diaryl allylic alcohols is described. The established protocol provides facile access to alpha-aryl-beta-oxyalkylated carbonyl ketones via radical addition and a 1,2-aryl migration cascade process. An application of the product has been demonstrated in the synthesis of a serotonin antagonist.
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