期刊
CHEMICAL COMMUNICATIONS
卷 49, 期 88, 页码 10382-10384出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c3cc46146g
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The methoxyamine group represents an ideal protecting group for the nitroxide moiety. It can be easily and selectively introduced in high yield (typically >90%) to a range of functionalised nitroxides using FeSO4 center dot 7H(2)O and H2O2 in DMSO. Its removal is readily achieved under mild conditions in high yield (70-90%) using mCPBA in a Cope-type elimination process.
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