期刊
CHEMICAL COMMUNICATIONS
卷 46, 期 43, 页码 8246-8248出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/c0cc03336g
关键词
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资金
- Ministry of Education, Culture, Sports and Technology (MEXT), Japan
- Shorai Foundation for Science
- Takeda Science Foundation
A catalytic domino reaction producing substituted 2-alkylidene-cyclohexanone from 3-oxymethyl-2-siloxy-1,3-butadienes, which can be prepared from Baylis-Hillman adducts, and alpha, beta-unsaturated ketones is described. The process involves two mechanistically distinct reactions, (4+2) cycloaddition and elimination. Both of these reactions are catalyzed by Tf2NH.
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