期刊
CHEMICAL COMMUNICATIONS
卷 46, 期 15, 页码 2641-2643出版社
ROYAL SOC CHEMISTRY
DOI: 10.1039/b926965g
关键词
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资金
- Ministry of Education, Culture, Sports, Science, and Technology, Japan
- KAKENHI
- Tohoku University Global COE program 'International Center of Research and Education for Molecular Complex Chemistry'
- Kato Memorial Bioscience Foundation
- [20390003]
A concise total synthesis of PDE-II featuring copper-mediated double aryl amination with the combination of CuI, CsOAc, and Cs(2)CO(3) is described. The highly substituted pyrroloindole skeleton was constructed by a one-pot five-step sequence including double aryl amination, beta-elimination, deprotection of a Cbz group, and removal of an Ns group followed by rearomatization.
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