☆ 4.7 Article

Nano-sized spinel LiMn2O4 powder fabricated via modified dynamic hydrothermal synthesis

CERAMICS INTERNATIONAL (2013)

期刊

CERAMICS INTERNATIONAL

卷 39, 期 3, 页码 3359-3364

出版社

ELSEVIER SCI LTD

DOI: 10.1016/j.ceramint.2012.07.093

关键词

Spinel LiMn2O4; Dynamic hydrothermal synthesis; Nano-particles

类别

Materials Science, Ceramics

资金

International Science and Technology Cooperation Program of China [2012DFG42100]
Doctoral Program of Higher Education of China [2011010113003]
Zhejiang Provincial Natural Science Foundation of China [LQ12B01003]
Zhejiang University of Technology [101009529]
National Natural Science Foundation of China (NSFC) [20506024]
State Key Development Program for Basic Research of china [2007CB216409]

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Protocol

Reagent

摘要

Nano-sized spinel LiMn2O4 powder with high crystallinity was prepared by a modified dynamic hydrothermal route. The as-synthesized LiMn2O4 powder exhibited high phase purity and better electrochemical properties than the material obtained via the static hydrothermal synthetic route. The dynamic method is believed to promote the simultaneous nucleation and growth of the LiMn2O4 phase during the synthesis. (C) 2012 Elsevier Ltd and Techna Group S.r.l. All rights reserved.

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