期刊
CERAMICS INTERNATIONAL
卷 38, 期 6, 页码 4943-4951出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.ceramint.2012.02.087
关键词
Calcination; Precursors: organic; Sintering; Nanocomposites; CeO2; Transition metal oxides
In this study, a new method to synthesize neodymium doped ceria ceramic nanopowders by the electrospinning of the hybrid polymers solution of their composite precursor was put forward. Calcined and sintered nanopowders were characterized by FT-IR, XRD, BET, SEM, and AFM techniques. According to the XRD analysis, the obtained powders are single phase and independent of the dopant concentration in the range investigated. The crystallite sizes were calculated using Scherrer equation. Moreover, lattice parameters, dislocation densities and microstrain values were calculated. BET results show that the increase of the neodymium doped content decrease the surface area of the composite powders, confirming the highly ordered micro and mesostructure. SEM and AFM results show that the samples have spherical grains. According to the surface roughness measurements, the increase in the amount of neodymium and the decrease in the amount of cerium decreased the surface roughness. (C) 2012 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
作者
我是这篇论文的作者
点击您的名字以认领此论文并将其添加到您的个人资料中。
推荐
暂无数据