期刊
CARBOHYDRATE RESEARCH
卷 343, 期 13, 页码 2215-2220出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.carres.2008.04.029
关键词
nitrone; necine bases; iminosugars; 1,3-dipolar cycloaddition
资金
- Ministry of Science and High Education [3 T09A 025 28]
The 1,3-dipolar cycloaddition of cyclic nitrone derived from tartaric acid and (S)-5-hydroxymethyl-2(5H)-furanone leads to a single adduct which was transformed into 2,6-dihydroxyhastanecine via reaction sequence involving reduction of the lactone moiety, glycolic cleavage of the terminal diol, and the N-O hydrogenolysis followed by the intramolecular alkylation of the nitrogen atom. (C) 2008 Elsevier Ltd. All rights reserved.
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