期刊
CARBOHYDRATE POLYMERS
卷 99, 期 -, 页码 166-172出版社
ELSEVIER SCI LTD
DOI: 10.1016/j.carbpol.2013.08.023
关键词
Hybrids; Cellulose; AgCl; Ag; Ultrasound; Antimicrobial activity
资金
- Fundamental Research Funds for the Central Universities [JC2013-3, TD2011-11]
- Beijing Nova Program [Z121103002512030]
- Program for New Century Excellent Talents in University [NCET-11-0586]
- National Natural Science Foundation of China [31070511, 51102172]
- Natural Science Foundation of Hebei Province [E2012210015]
This study aims to investigate the fabrication and property of cellulose/Ag/AgCl hybrids. In this article, preparation of cellulose/Ag/AgCl hybrids was reported using the cellulose solution, AgNO3, AlCl3 center dot 6H(2)O with ultrasound agitation method. The cellulose solution was synthesized by the dissolution of the microcrystalline cellulose in NaOH/urea aqueous solution. Influences of the experimental parameters of ultrasound treatment time and ultrasonic intermittent on the hybrids were investigated. The phase, microstructure, thermal stability, and morphology of the hybrids were characterized by X-ray powder diffraction (XRD), Fourier transform infrared (FTIR) spectrometry, thermogravimetric analysis (TGA), differential thermal analysis (DTA), and scanning electron microscopy (SEM). Results showed the successful synthesis of cellulose/Ag/AgCl hybrids with good thermal stability. Moreover, the hybrids displayed desirable antimicrobial activities. Compared with other conventional methods, the rapid, green, and environmentally friendly ultrasound agitation method opens a new window to the high value-added applications of biomass. (C) 2013 Elsevier Ltd. All rights reserved.
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