Crystal structure of semiorganic antimony thiourea bromide monohydrate crystals: a redetermination

The growth of antimony thiourea bromide monohydrate (ATBM) single crystals by evaporation technique at room temperature is reported here. Antimony thiourea bromide monohydrate crystallizes in the orthorhombic space group Cmca with unit cell parameters a = 12.320(7) angstrom, b = 11.668(7) angstrom, c = 18.615(11), and z = 8. The structure has been solved by direct methods and refined to a final R value of 0.0239.