期刊
BULLETIN OF MATERIALS SCIENCE
卷 36, 期 1, 页码 153-156出版社
INDIAN ACAD SCIENCES
DOI: 10.1007/s12034-013-0428-5
关键词
Continuous gel fibre; sol-gel method; Al2O3; polyvinylpyrrolidone
资金
- Shaanxi Natural Science Foundation of China [2012JQ6017]
- Shaanxi University of Technology Foundation of China [SLGQD1101]
Continuous alumina gel fibres were prepared by sol-gel method. The spinning sol was prepared by mixing aluminum nitrate, lactic acid and polyvinylpyrrolidone with a mass ratio of 10:3:1 center dot 5. Thermogravimetry-differential scanning calorimetry (TG-DSC), Fourier transform infrared (FTIR) spectra, X-ray diffraction (XRD), and scanning electron microscopy (SEM) were used to characterize the properties of the gel and ceramic fibres. The Al2O3 fibres with a uniform diameter can be obtained by sintering gel fibres at 1200 A degrees C.
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