期刊
JOURNAL OF ANALYTICAL CHEMISTRY
卷 71, 期 1, 页码 82-93出版社
PLEIADES PUBLISHING INC
DOI: 10.1134/S1061934815120035
关键词
pesticides; food; feed; water; soil; grain; high-performance liquid chromatography; high-resolution time-of-flight mass spectrometry
A method has been proposed for the simultaneous identification and determination of 111 pesticides from various classes in food by high-performance liquid chromatography-high-resolution time-offlight mass spectrometry combined with simple and fast sample preparation. Possibility of the identification and determination of pesticides in drinking, natural, and ground waters without sample preparation has been demonstrated. A scheme of the identification and determination of the detected analytes using the standard addition method has been suggested. The limit of detection is 0.05 (0.1) A mu g/(L)kg. The relative standard deviation of the results of analysis does not exceed 0.1. The time of identification is 30-40 min and time of determination is 1-2 h.
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