期刊
APPLIED ORGANOMETALLIC CHEMISTRY
卷 28, 期 8, 页码 635-640出版社
WILEY
DOI: 10.1002/aoc.3173
关键词
beta-CD-capped Pd-0 nanoparticles; beta-cyclodextrin/N-methylurea mixture; ligand-free
Low-melting beta-cyclodextrin/N-methylurea (NMU) mixture, an efficient catalytic system for ligand-free Suzuki and Heck couplings in the presence of fresh native beta-CD-capped Pd-0 nanoparticles, has been successfully reported. This natural and convenient system can be performed in air and could afford the corresponding cross-coupled products in good to excellent isolated yields after a simple workup under every low Pd loading (0.05 mol%). Remarkably, the catalytic system can be recycled and reused without loss of catalytic activity. Copyright (C) 2014 John Wiley & Sons, Ltd.
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